GCMS comments for sample AD26473 detecting N,N-dimethylbenzenesulfonamide

NYC 911 Public Portal Document ! Am Deviewed)

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3001\26473.D Vial: 9 Acq On : 30 Nov 2001 7:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins 2 Multiplr: 1.00 Mise MS Integration Params: RTEINT.P Quant Time: Dec 3 14:54 2001 Quant Results File: NP112701.RES Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701 4 3 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) ,4-Dichlorobenzene-d4 11.89 152 1373269 20.00 ng/uL -0.04 19) aphthalene-d8 15.50 136 5372001 20.00 ng/uL -0.04 31) cenaphthene-dlO 20.78 164 2435459 20.00 ng/uL -0.04 49) henanthrene-d10 25.19 188 3477955 20.00 ng/uL -0.05 59) hrysene-d12 33.19 240 2175560 20.00 ng/uL -0.05 68) erylene-d12 37.27 264 1570956 20.00 ng/uL -0.06 SysteMonitoring Compounds 4) Fluorophenol 0.00 112 0 0.00 ng/uL Spid Amount 75.000 Range 18 42 Recovery 0.00%# 5) enol-d5 0.00 99 0 0.00 ng/uL Spid Amount 75.000 Range 19 32 Recovery = 0.00%# 6) Zhlorophenol-d4 11.89 132 1129 0.01 ng/uL 0.47 Spil Amount 75.000 Range 34 84 Recovery- S 0.01%# 7) $-Dichlorobenzene-d4 12.41 152 14548 0.25 ng/uL -0.05 Spik Amount 50.000 Range 26 73 Recovery 0.50%# 20) robenzene-d5 0.00 82 0 0.00 ng/uL Spik Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2uorobiphenyl 18.92 172 4775 0.03 ng/uL 0.09 Sp ikAmoun t 50.000 Range 42 78 Recovery = 0.06%# 33) 26-Tribromophenol 0.00 330 0 0.00 ng/uL Sp ikAmount 75.000 Range 45 96 Recovery 5 0.00%# 62) Tienyl-d14 0.00 244 0 0.00 ng/uL Sp ikmount 50.000 Range 58 98 Recovery 0.00%# Targetpounds Qvalue 2) Pine 0.00 79 0 N.D. 3) Ncosodimethylamine 0.00 74 0 N.D. 8) Pi. 0.00 94 0 N.D. 9) bichloroethyl) ether 0.00 93 0 N.D. 10) 2-rophenol 0.00 128 0 N.D. 11) 1 chlorobenzene 0.00 146 0 N.D. 12) 1, chlorobenzene 0.00 146 0 N.D. 13) 1,hlorobenzene 0.00 146 0 N.D. 14) 2-lphenol 0.00 108 0 N.D. 15) 2,ybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&hylphenol 0.00 108 0 N.D. 17) N-odi-n-propylamine 0.00 70 0 N.D. 18) Herroethane 0.00 117 0 N.D. 21) Nitzene 0.00 77 0 N.D. 22) ISe 0.00 82 0 N.D. 3 2

#) = @ur out of range (m) = manual integration 6473.D '701.M Tue Dec 04 08:24:00 2001

NYC-WTC_000031638