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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document (o Reviewed) Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\NOV3 001\26388.D Vial: 14 Acq On 1 Dec 2001 12:02 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 3 15:24 2001 Quant Results File: NP112701.RES Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.89 152 1448612 20.00 ng/uL -0.05 19) Naphthalene-d8 15.50 136 5622454 20.00 ng/uL -0.05 31) Acenaphthene-diO 20.78 164 2508790 20.00 ng/uL -0.04 49) Phenanthrene-diO 25.19 188 3641229 20.00 ng/uL -0.05 59) Chrysene-dl2 33.19 240 2317715 20.00 ng/uL -0.06 68) Perylene-dl2 37.28 264 1660070 20.00 ng/uL -0.06 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 - 42 Recovery = 0.00%# 5) Phenol -d5 11.15 99 884 0.01 ng/uL 0.02 Spiked Amount 75.000 Range 19 32 Recovery = 0.01%# 6) 2-Chlorophenol-d4 11.90 132 1567 0.02 ng/uL 0.47 Spiked Amount 75.000 Range 34 84 Recovery = 0.03%# 7) l,2-Dichlorobenzene-d4 12.41 152 14251 0.23 ng/uL -0.05 Spike Amount 50.000 Range 26 73 Recovery = 0.46%# 20) Nirobenzene-d5 0.00 82 0 0.00 ng/uL Spike Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2 -luorobiphenyl 18.92 172 4818 0.03 ng/uL 0.09 Spike Amount 50.000 Range: 42 78 Recovery = 0.06%# 33) 2,, 6 -Tribromophenol 0.00 330 0 0.00 ng/uL Spike; Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Tehenyl-d14 0.00 244 0 0.00 ng/uL Spike Amount 50.000 Range 58 98 Recovery = 0.00%# Target pounds Qvalue 2) Pydine 0.00 79 0 N.D. 3) N-trosodimethylamine 0.00 74 0 N.D. 8) Phol 0.00 94 0 N.D. 9) bi?-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-torophenol 0.00 128 0 N.D. 11) 1, Jichlorobenzene 0.00 146 0 N.D. 12) 1, ichlorobenzene 0.00 146 0 N.D. 13) 1, ichlorobenzene 0.00 146 0 N.D. 14) 2-mylphenol 0.00 108 0 N.D. 15) 2, bxybis (1-Chloropropan 12.90 45 3149 N.D. 16) 3&4thylphenol 0.00 108 0 N.D. 17) N-Nosodi-n-propylamine 0.00 70 0 N.D. 18) Hexloroethane 0.00 117 0 N.D. 21) Nitenzene 0.00 77 0 N.D. 22) Isotone 0.00 82 0 N.D. je 2

#) = quiier out of range (m) = manual integration >6388.D .12701.M Tue Dec 04 08:19:40 2001 Page 1

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NYC-WTC_000031454Source: NYC Law Department, mirrored locally

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