GCMS analysis result with unknowns, Dec 2001

NYC 9/11 Public Portal Document AH (OT Reviewed)

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3001\26335.D Vial: 17 Acq On : 1 Dec 2001 2:45 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise t Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 3 15:25 2001 Quant Results File: NP112701.RES Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 11.89 152 1483176 20.00 ng/uL -0.04 19) Naphthalene-d8 15.50 136 5720244 20.00 ng/uL -0.04 31) Acenaphthene-diO 20.78 164 2540784 20.00 ng/uL -0.04 49) Phenanthrene-diO 25.19 188 3660446 20.00 ng/uL -0.05 59) Chrysene-dl2 33.19 240 2358320 20.00 ng/uL -0.05 68) Perylene-dl2 37.28 264 1775963 20.00 ng/uL -0.05 {stem Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.90 132 1232 0.01 ng/uL 0.48 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 12.41 152 14612 0.23 ng/uL -0.04 Spiked Amount 50.000 Range 26 73 Recovery = 0.46%# 0) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 2) 2-Fluorobiphenyl 18.92 172 4825 0.03 ng/uL 0.09 Spiked Amount 50.000 Range 42 - 78 Recovery = 0.06%# 3) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 - 96 Recovery = 0.00%# 2) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 - 98 Recovery = 0.00%# get Compounds Qvalue ) Pyridine 0.00 79 0 N.D. ) N-nitrosodimethylamine 0.00 74 0 N.D. ) Phenol 0.00 94 0 N.D. ) bis(2-Chloroethyl)ether 0.00 93 0 N.D. ) 2 1Chiorophenol 0.00 128 0 N.D. ) 1,3-Dichlorobenzene 0.00 146 0 N.D. ) 1,4-Dichlorobenzene 0.00 146 0 N.D. ) 1,2-Dichlorobenzene 0.00 146 0 N.D. ) 2-Methylphenol 0.00 108 0 N.D. t 2,2 ' -oxybis (1-Chloropropan 0.00 45 0 N.D. 3 &4-Methylphenol 0.00 108 0 N.D. N-Nitrosodi-n-propylamine 0.00 70 0 N.D. Hexachloroethane 0.00 117 0 N.D. Nitrobenzene 0.00 77 0 N.D. ge 2 Isophorone 0.00 82 0 N.D. = qualifier out of range (m) = manual integration 5.D 1 NP112701.M Tue Dec 04 14:24:27 2001 Page 1

NYC-WTC_000031374