GCMS analysis results for sample AD26319, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC0501\26319.D Vial: 7 . Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 5 15:06 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Interna.1 Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.87 152 1008535 20.00 ng/uL -0.07 19) Naphthalene-d8 15.48 136 3735013 20.00 ng/uL -0.07 31) Acenaphthene-dlO 20.75 164 1684867 20.00 ng/uL -0.07 49) Phenanthrene-dlO 25.16 188 2354953m 20.00 ng/uL -0.08 59) C’hrysene-dl2 33.17 240 1447812 20.00 ng/uL -0.08 68) Perylene-dl2 37.25 264 993984 20.00 ng/uL -0.09

System Monitoring Compounds 4) 2 - Fluorophenol 0 . 00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.88 132 324 0.00 ng/uL 0.45 Spiked Amount 75.000 Range 34 84 Recovery = 0.00%# 7) 1,2-Dichlorobenzene-d4 12.02 152 3219 0.08 ng/uL -0.44 Spiked Amount 50.000 Range 26 73 Recovery = . 0.16%# 20) Mitrobenzene-d5 0 . 00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.90 172 1891 0.02 ng/uL 0.07 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75 . 000 Range • 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL .Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0 . 00 123 0 N.D. 11) 1,3-Dichlorobenzene 0.00. 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0 . 00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2 ‘ -oxybis (1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 103 0 N.D. 17) N-Nitrosodi-n-propylamine 13.19 70 288 N.D. 18) Hexachloroethane 0 . 00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 26319.D NP112701.M Wed Dec 05 15:06:41 2001 Page 1

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