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GCMS analysis results for sample AD26319, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26319 with unidentified compounds detected.

NYC-WTC_000031297–000031318

Folder label: “GCMS X 11/3/01 A 12/1/01

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Scanned page image, NYC-WTC_000031313
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compo: Report Data File C : \HPCHEM\1\DATA\DEC0501‘ 319 .D vial: 7 Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 I n~t : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C: \HPCHEM\1\METHODS\‘ 2701.M (RTE Integrator) Title 208 625/TCLP calibra: .’ table Library C:\DATABASE\NBS7SK.L ************************************** • ' **************************** Peak Number 10 1-Monolinoleoylglycern" rimet Concentration Rank 9

R.T. EstConc Area ative to ISTD R.T.

28.81 0.94 ng/uL 339844 p: nthrene-d10 25.16

Hit# of 5 Tentative ID J MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethyls; 1 C27H5404Si2 054284-45-6 33 2 Benzoic acid, 2,4-bis [ ( trimethylsi ' 1 C16H3004Si3 010586-16-0 25 3 3 - Isopropoxy -1,1, 1,7,7,7 -hexamethy 5 C18H5207Si7 071579-69-6 25 4 N-(Trifluor Abundance C 1)-0 acetyScan ,0',0"- tri5(tr; 2614 (28.814 min): 26319.D (-) — C20H36F3NO4Si3 000000-00-0 17 m/ z 73.05 100.00% 73

5000 147 221 355 Z................. 281 28.40 28.60 28.80 29.00 29.20 । 45 117 1 191+L 249 , j 325 i 401 4? 500 550 m/z 147.10 32.42% m/z-> 5'3 100 150 200 250 300| 350 400 Abundance .758871: 1-Monolinoleoylglycerol trmethylsil. 73

207 — -............ 5000 147 28.40 28.66 28.80 29.00 29.20 34 103 ! , 281 m/z 355.05 19.89%

m/z-> 50 100 .... LLL X 150 200 250 300__ 350 400 32 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethyisily!)oxy. 73 ..r 28 40 28.50 28.80 29.00 29.20 5000 355 m/z 2 2... . 05 19.45% . 45

133 193 2?3 281 * m/z->__ Abundance I 50

73 100 150 200 250 300 350 #60503: 3-Isopropoxy-1 ,1,1,7,7,7-hexamethyl-3,5 .. ' 400 n 500 550 r,-m TTt M.. 28.40 28.60 28.80 29.00 29.20 m/z 2 81.6.0 14.82% | 5000 147

221 281 327 41: 1, i 519 561 I ' ' 1 ' I 1 ' 1 1 1 1 1 1 1 1 m/z-> 50 100 150 200 250 300 330 400 509 550 28 40 28.60 28.80 29.00 29.20

26319.D NP112701.M Wed Dec 05 1’ 6 2001 Page 10

NYC-WTC_000031313

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NYC-WTC_000031313Source: NYC Law Department, mirrored locally

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