NYC-WTC_000030836
Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis results for sample AD26319, Dec 2001
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AD26319 with unidentified compounds detected.
NYC-WTC_000031297–000031318Folder label: “GCMS X 11/3/01 A 12/1/01”
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NYC 9/11 Public Portal Document
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Data File C:\HPCHEM\1\DATA\DEC0501’. 319.D Vial: 7 Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 I ns t : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\N. 2701.M (RTE Integrator) Title 208 625/TCLP calibras: . table Library C:\DATABASE\NBS75K.L *************** ***************** * ***** **************************** Peak Number 8 Benzoic acid, 2,5-bis( methy Concentration Rank 4
R.T. EstConc Area ative to I STD R.T.
22 . 97 2.67 ng/uL 963920 Pi.. -ithrene-dlO 25.16
Hit# of 5 Tentative ID ”T MolForm CAS# Qual
1 Benzoic acid, 2,5 bis ( trimethy Isil F 0 C16H30O4Si3 003618-20-0 47 2 N- (Trif luoroacecyl) -0,0 ' , 0 ' 1 - tris (: 1 C19H34F3NO4Si3 000000-00-0 37 3 N- (Trifluoracetyl) -0,0' , 0"-tris (tri 3 C20H36F3NO4Si3 000000-00-0 37 4 Benzeneethazamine, N- [(pentafluorc 3 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1977 (22.973 min): 26c : 9.D (•) in/z 73 . 05 100.00% 70
5000 147 355 221 281 22.60 22.80 23.00 23.20 23.40 45 117 191 , . 249 . ( 227—1 m/z 355.05 28.89% m/z->50 100 150 200 250 300 350 450 500 Abundance #7 3978: Benzoic acid, 2,5-bis(trimethylsloxy)-, i 73 355
......................... / 5000 22.60 22.80 23.00 23.20 23.40 45 "z 147.00 25.13%
n/z-> 4 T1I ~ 50 100 ' 47 1 79 150 200 223 , 250 267 297 300 350 450 500 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tn'(!!imeth’.'. 73 355 TT T 1 IT 22.60 22.80 23.00 23.20 23.40 5000 m/z 221.05 18.26%
45 ■ 1 1 _1 126147 • ■ 1 ■ i ' 193 265 ' I ■ 481 ' ' ' i ■ m/z->______ 50_____ 100 150 200 250 300 350 450 500 Abundance # 58807: N-(Trilluoracetyl)-O,0 ‘,O"-trisstrimethyisit 2 ________ __ rl 1 1 • • i • ■ ■ ■ i • ■ ■ • i > 70 22 60 22.80 23.00 23.20 23.40 355 m/z 2 81.00 15.08% 5000 ft 45 281 Ii 140 ' । ■ --HT 184 480 ' i 1 • 1 1 i ' TT ‘II I It m/z--> 50 100 150 200 250 300 350 450 500 22.60 22.80 23.00 23.20 23.40
26319.D NP112701.M Wed Dec 05 15 :34 2001 Page 8 NYC-WTC_00003131 1
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NYC-WTC_000031311Source: NYC Law Department, mirrored locally
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