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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DECO401\26205.D Vial: 68 Acq On 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 6.424 147 150 161 rVV 37613 104403 1.07% 0.169% 2 7.021 211 215 225 rBV 134318 272165 2.80% 0.439% 3 7.682 280 287 306 rBV 557770 1421221 14.63% 2.294% 4 11.152 659 665 672 rBV 53354 136935 1.41% 0.221% 5 11.565 701 710 713 rBV 70959 171064 1.76% 0.276% 6 11.703 719 725 736 rBV 2322686 5654536 58.22% 9.128% 7 11.831 736 739 751 rVB 56928 146570 1.51% 0.237% 8 12.116 765 770 775 rBV 65775 144479 1.49% 0.233% 9 12.538 807 816 820 rBV 50508 146034 1.50% 0.236% 10 14.338 1003 1012 1019 rBV 460937 972039 10.01% 1.569% 11 15.311 1111 1118 1136 rBV 3360372 7588947 78.14% 12.251% 12 17.477 1346 1354 1364 rBV 1067488 2266137 23.33% 3.658% 13 18.175 1423 1430 1436 rBV 127228 249057 2.56% 0.402% 14 20.296 1653 1661 1668 rBV 886924 1874337 19.30% 3.026% 15 20.589 1686 1693 1707 rBV 3476784 7830992 80.63% 12.642%

16 21.030 1736 1741 1752 rBV 210342 438132 4.51% 0.707% 17 22.811 1929 1935 1948 rBV 621471 1307172 13.46% 2.110% 18 25.005 2165 2174 2187 rBV2 3217494 7990784 82.27% 12.900% 19 26.905 2375 2381 2388 rBV 318970 645661 6.65% 1.042% 20 28.668 2567 2573 2582 rBV 245976 529017 5.45% 0.854% 21 30.265 2739 2747 2753 rBV 215951 459988 4.74% 0.743% 22 31.725 2900 2906 2915 rVB 194262 433419 4.46% 0.700% 23 33.038 3040 3049 3054 rBV2 2359922 5517106 56.80% 8.906% 24 33.102 3054 3056 3069 rVB 217435 451612 4.65% 0.729% 25 34.387 3188 3196 3203 rBV 149558 381144 3.92% 0.615% 26 35.590 3320 3327 3347 rBV 4002867 9712377 100.00% 15.679% 27 36.728 3444 3451 3460 rBV 77941 245675 2.53% 0.397% 28 37.132 3487 3495 3514 rBV2 1620828 4591260 47.27% 7.412% 29 38.032 3586 3593 3602 rBV3 41590 159337 1.64% 0.257% 30 39.611 3756 3765 3777 rBV4 21811 104861 1.08% 0.169%

NYC-WTC 000031136

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NYC-WTC_000031136Source: NYC Law Department, mirrored locally

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