GCMS analysis results for sample AD26132, Dec 2001

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Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3001\26132.D Vial: 64 Acq On 1 Dec 2001 4:22 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 1 5:11 2001 Quant Results File: NP112601.RES Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 09:03:50 2001 Response via : Initial Calibration DataAcq Meth : NP112601

Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 715969 20.00 ug/1 0.00 19) Naphthalene-d8 15.31 136 2751431 20.00 ug/1 0.00 31) Acenaphthene-d10 20.58 164 1279265 20.00 ug/l 0.00 49) Phenanthrene-d10 25.00 188 1754512 20.00 ug/l 0.00 59) Chrysene-d12 33.03 240 1097737 20.00 ug/1 0.00 68) Perylene-d12 37.13 264 748695 20.00 ug/l 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/l Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/l Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.69 132 699 0.01 ug/1 0.49 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.22 152 8366 0.28 ug/l 0.00 Spiked Amount 50.000 Recovery = 0.56% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/l Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.73 172 2779 0.04 ug/1 0.15 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/l Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-d14 0.00 244 0 0.00 ug/l Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 26132.D NP112601.M Mon Dec 03 12:07:57 2001 Page 1

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