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Spiked sample analysis AD27009, Nov-Dec 2001

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DEP laboratory spiked sample analysis (SS525) for sample AD27009 conducted between November 13 and November 30, 2001.

NYC-WTC_000030557–000030561

Folder label: “525 11/13/01 - 11/30/01 12/6 12/17 12/20/01

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2 2 K K 0 o 3 o — 0 1 "0 C 0 0 0 0 Integration Report Quanfile: 27009MS Quan Entries: 28 O o C 0 Connent: BOHLK: METHOD 525; INST 204; 11/30/01; SAMPLE 27009 MS "0 0 C CD Sorted via: Entry Nunber 1 — 0 0 0 No Name of Compound R Tine Scan# Node Peak Area Pk Height 0 0 C 3 0 3 chrysene d-12(IS) 22:37 1357 Auto 3,386,104 1,364,879 D

4 p-terphenyl d-14(IS) 20:47 1247 Auto 6,212,288 3,970,359 5 acenaphthene d-10(SURR 12:13 733 Auto 2,658,939 1,430,818 6 phenanthrene d-10(SURR 16:49 1009 Auto 4,018,159 1,578,574 7 chrysene d-12 (SURR) 22:37 1357 Auto 3,386,104 1,364,879 8 1,3-d imethy1-2-n itrobe 7:55 475 Auto 1,320,715 729,736 9 triphenyl phosphate (S 22:02 1322 Auto 1,807,679 1,017,628 10 perylene d-12 CSURR) 26:51 1611 Auto 1,997,549 419,732 11 hexach lorocyc lopentad i 10:05 605 Auto 298,049 149,012 12 hexach lorobenzene 15:14 914 Auto 1,253,022 544,444 13 sinazine 16:01 961 Auto 727,303 206,884 14 atrazine 16:11 971 Auto 802,736 275,359 15 alachlor 18:20 1100 Auto 1,442,981 807,244 16 bis(2~ethyihexyI Jadipa 21:55 1315 Auto 2,141,778 1,365,000 17 bisC2-ethyIhexyl phtha 22:54 1374 Auto 4,933,806 2,368,285 18 benzo(a)pyrene 26:37 1597 Auto 2,389,779 500,045 19 eptc 10:30 630 Auto 5,162,556 2,689,738 20 2,6-d in itrotoluene 11:52 712 Auto 783,035 307,149 21 2,4-dinitrotoluene 12:51 771 Auto 816,261 405,044 22 no1 inate 12:59 779 Auto 1,995,895 1,079,130 23 terbac i1 17:21 1041 Auto 1,581,541 443,763 24 acetochlor 18:08 1088 Auto 953,894 587,650 25 metribuzin 18:10 1090 Auto 962,058 471,022 26 metolachlor 19:05 1145 Auto 4,389,578 2,317,323 27 butachlor 20:19 1219 Auto 982,354 540,937 28 4,4* -dde 20:43 1243 Auto 1,479,279 1,130,902

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NYC-WTC_000030560Source: NYC Law Department, mirrored locally

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