NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\121901\1217MDL.D Vial: 39
Acq On : 20 Dec 2001 5:49 pm Operator: McLean
Sample : 12/17 fblks study Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: BENZO.P
Quant Time: Dec 20 18:26:32 2001 Quant Results File: 121401.RES
Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator)
Title : Quantitation For Method 525.2
Last Update : Tue Dec 18 09:35:41 2001
Response via : Initial Calibration
DataAcq Meth : 121401
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-dlO 18.20 164 2179771 5.00 ug/L 0.00 MDU
9) Phenanthrene D-10 22.53 188 3246994 5.00 ug/L 0.00
20) Chrysene D-12 30.30 240 1862802 5.00 ug/L 0.00
System Monitoring Compounds
2) 1,3-Dimethyl-2-nitrobenzen
Spiked Amount 5.000
19) Triphenyl Phosphate surr
Spiked Amount 5.000
13.13
29.58
134
326
425202
Recovery
460926
Recovery
3.81 ug/L
= 76.20%
4.66 ug/L
= 93.20%
0.00
0.00 FB ‘s
21) Perylene D-12 surr 34.32 264 969435 3.94 ug/L 0.00
Spiked Amount 5.000 Recovery = 78.80%
Target Compounds Qvalue
3) Hexachlorocyclopentadiene 15.37 237 0 N.D.
4) Hexachlorobenzene 21.40 284 25403 0.18 ug/L 90
5) EPTC 16.18 128 153530 0.74 ug/L 100
6) 2,6-Dinitrotoluene 17.78 165 57256 0.82 ug/L 85
7) 2,4-Dinitotoluene 18.93 165 27280 0.51 ug/L 94
8) Molinate 19.09 126 267195 0.91 ug/L 93
10) Simazine 22.49 201 1829m 0.02 ug/L
11) Atrazine 22.05 200 10591 0.09 ug/L 98
12) Alachlor 23.91 160 19700 0.18 ug/L # 71
13) Terbacil 22.83 161 103773 1.20 ug/L 90
14) Acetochlor 23.69 146 140984 1.73 ug/L 94
15) Metribuzin 23.74 198 3672m 0.20 ug/L
16) Metolachlor 24.84 162 58326 0.16 ug/L 96
17) Butachlor 26.65 160 27138 0.26 ug/L # 37
18) 4,4'-DDE 27.29 246 72481 0.57 ug/L 92
22) Bis (2-Ethylhexyl) adipate 29.52 129 15498 0.43 ug/L 87
23) Bis (2-Ethylhexyl) phthala 30.96 149 271841 0.82 ug/L 93
24) Benzo (a) pyrene 34.17 252 19562 0.05 ug/L 95
(#) = qualifier out of range (m) = manual integration
1217MDL.D 121401.M Wed Jan 02 09:34:50 2002 Page 1
NYC-WTC_000030550
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