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Spiked sample analysis AD27009, Nov-Dec 2001

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DEP laboratory spiked sample analysis (SC1525) for sample AD27009 conducted on November 30, 2001.

NYC-WTC_000030535–000030551

Folder label: “525 11/13/01 - 11/30/01 12/6 12/17 12/20/01

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Z 2 K O o co _s

O U I o o o Integration Report Quanfile: MDL1206 Quan Entries: 28 C O o o C Connent: BOHLK; METHOD 525; INST 204; 12/06/01; MDL "0 o o CH Sorted via: Entry Nunber 1 — 9 00 oo No Name of Compound R Tine Scant Node Peak Area Pk Height O C 3 CD 3 chrysene d-12(IS) 22:34 1354 Auto 4,075,751 1,883,172 4 p-terphenyl d-14CIS) 22:34 1354 Auto 4,075,751 1,883,172 5 acenaphthene d-10(SURR 12:11 731 Auto 3,423,551 2,316,193 6 phenanthrene d-10(SURR 16:46 1006 Auto 4,875,392 1,914,470 7 chrysene d-12 (SURR) 22:34 1354 Auto 4,075,751 1,883,172 8 1,3-d inethy1-2-n itrobe 7:53 473 Auto 1,667,146 862,109 9 triphenyl phosphate (S 22:00 1320 Auto 2,166,665 1,334,375 10 perylene d-12 CSURR) 26:45 1605 Auto 2,662,697 562,789 11 hexach lorocyc lopentad i 10:03 603 Auto 23,862 12,002 12 hexachlorobenzene 15:11 911 Auto 79,833 31,008 13 sinazine 15:58 958 Auto 22,029 4,258 14 atrazine 16:07 967 Auto 31,082 9,473 15 alachlor 18:17 1097 Auto 76,164 38,539 16 bis (2-ethyIhexyl)ad ipa 21:53 1313 Auto 131,628 66,417 17 bis (2-ethy Ihexy l phtha 22:51 1371 Auto 773,409 324,003 18 benzo(a)pyrene 26:32 1592 Auto 89,139 16,502 19 eptc 10:28 628 Auto 1,135,141 539,050 20 2,6-d in itrotoluene 11:50 710 Auto 246,878 134,406 21 2,4-d in itrotoluene 12:50 770 Auto 380,948 82,940 22 no1 inate 12:56 776 Auto 523,798 252,368 23 terbac i1 17:15 1035 Auto 525,419 160,302 24 acetochlor 18:06 1086 Auto 428,706 195,707 25 netribuzin 18:08 1088 Auto 54,652 21,673 26 netolachlor 19:03 1143 Auto 221,098 110,457 27 butachlor 20:18 1218 Auto 97,813 62,666 28 4,4*-dde 20:41 1241 Auto 305,743 233,103

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NYC-WTC_000030548Source: NYC Law Department, mirrored locally

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