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← Document results/DEP Box 20/525 X 11/14, 11/19, 12/7, 12/17 A 12/1/01 12/3/01 12/18/01 12/19/01
Document / 19 pages

Organic chemicals lab blank results, Nov-Dec 2001

Machine-extracted title · confidence 90%

Laboratory blank analysis report for organic chemicals at site 525 conducted between November and December 2001.

NYC-WTC_000030316–000030334

Folder label: “525 X 11/14, 11/19, 12/7, 12/17 A 12/1/01 12/3/01 12/18/01 12/19/01

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File C:\MSDCHEM\1\DATA\1219O1\CAL2A.D Vial: 3 Acq On 19 Dec 2001 1:43 pm Operator: McLean Sample 5.0 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO. P Quant Time: Dec 19 14:27:00 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 18 09:35:41 2001 Response via : Initial Calibration DataAcq Meth : 121401

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.21 164 7953485 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 10903347 5.00 ug/L 0.00 20) Chrysene D-12 30.30 240 6926515 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1953603 4.80 ug/L 0.00 Spiked Amount 5.000 Recovery = 96.00% 19) Triphenyl Phosphate surr 29.58 326 1882002 5.67 ug/L 0.00 Spiked Amount 5.000 Recovery = 113.40% 21) Perylene D-12 surr 34.31 264 4687820 5.12 ug/L 0.00 Spiked Amount 5.000 Recovery = 102.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.71 237 1027054 4.56 ug/L 97 4) Hexachlorobenzene 21.40 284 2734229 5.20 ug/L 97 5) EPTC 16.18 128 4495956 5.94 ug/L 99 6) 2,6-Dinitrotoluene 17.77 165 2100636 5.50 ug/L 96 7) 2,4-Dinitotoluene 18.92 165 2482872 5.33 ug/L 99 8) Molinate 19.09 126 6365773 5.93 ug/L 97 10) Simazine 21.94 201 1791091 6.05 ug/L 98 11) Atrazine 22.06 200 2592202 6.69 ug/L 97 12) Alachlor 23.91 160 2376381 6.31 ug/L 90 13) Terbacil 22.89 161 2765506 6.34 ug/L 99 14) Acetochlor 23.70 146 1723481 6.29 ug/L 99 15) Metribuzin 23.74 198 2953410 5.68 ug/L 97 16) Metolachlor 24.84 162 7804163 6.43 ug/L 99 17) Butachlor 26.66 160 2286722 6.53 ug/L 87 18) 4,4'-DDE 27.29 246 2329554 5.49 ug/L 95 22) Bis (2-Ethylhexyl) adipate 29.52 129 6823604 5.72 ug/L 97 23) Bis (2-Ethylhexyl) phthala 30.96 149 10590586 4.95 ug/L 100 24) Benzo (a) pyrene 34.17 252 8294864 6.08 ug/L 97

(#) = qualifier out of range (m) = manual integration CAL2A.D 121401.M Wed Dec 19 14:27:01 2001 Page 1

NYC-WTC_000030328

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NYC-WTC_000030328Source: NYC Law Department, mirrored locally

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