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GCMS Spiked Sample Results, Nov 2001

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry results for spiked sample AD25843 including Hexachlorobenzene and phthalates from November 2001.

NYC-WTC_000030015–000030019

Folder label: “525 X 11/1/01 AN 11/16 - 11/17/01

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I o "0 o C o Integration Report Quanfile: 25843MS Quan Entries: 28 O o o O C Comment: BOHLK: METHOD 525; INST 204J 11/16/01; SAMPLE 25843 MS "0 O 0 o Sorted via: Entry Number T — 9 CO O No Name of Compound R Time Scani Node Peak Area Pk Height 0 O C 3 0 3 chrysene d-12(IS) 22:41 1361 Auto 1,914,526 839,367 D

4 p-terphenyl d-14(IS) 20:51 1251 Auto 235,833 94,155 5 acenaphthene d-10(SURR 12:18 738 Auto 1,856,749 966,223 6 phenanthrene d-10CSURR 16:56 1016 Auto 3,155,630 1,256,506 7 chrysene d-12 (SURR) 22:41 1361 Auto 1,914,526 839,367 8 1,3-d imethy1-2-nitrobe 7:58 478 Auto 1,216,510 674,144 9 triphenyl phosphate (8 22:06 1326 Auto 1,435,780 612,139 10 perylene d-12 CSURR) 26:59 1619 Auto 528,018 93,340 11 hexachlorocyclopentadi 10:09 609 Auto 207,807 121,954 12 hexachlorobenzene 15:21 921 Auto 1,133,814 471,317 13 simazine 16:06 966 Auto 636,502 190,000 14 atrazine 16:17 977 Auto 709,475 230,555 15 alachlor 18:24 1104 Auto 1,102,129 683,035 16 b is (2-ethy Ihexy Dad ipa 21:58 1318 Auto 1,175,310 389,733 17 b is(2-ethyihexy1 )phtha 22:58 1378 Auto 3,539,597 1,250,585 18 benzo (a pyrene 26:45 1605 Auto 631,957 106,652 19 eptc 10:33 633 Auto 5,018,239 2,689,840 20 2,6-d in itrotoluene 11:56 716 Auto 706,943 297,740 21 2,4-d in itrotoluene 12:55 775 Auto 772,930 350,892 22 molinate 13:03 783 Auto 2,057,995 1,327,500 23 terbac il 17:24 1044 Auto 1,128,551 379,417 24 acetochlor 18:12 1092 Auto 817,270 400,308 25 metribuzin 18:14 1094 Auto 771,083 334,195 26 metolachlor 19:09 1149 Auto 3,478,227 1,861,582 27 butachlor 20:23 1223 Auto 1,036,391 677,703 28 4,4"-dde 20:46 1246 Auto 1,330,486 1,066,964

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NYC-WTC_000030018Source: NYC Law Department, mirrored locally

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