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Method detection limit verification, sample AD25601, Nov 2001

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Laboratory report of method detection limit verification for sample AD25601 conducted November 13, 2001.

NYC-WTC_000029547–000029551

Folder label: “525 X 10/29/01 AN 11/13 - 11/14/01

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2 Z K o O 3 o _s

i o "0 C o o O Integration Report Quanfile: MDLB1113 Quan Entries: 28 O o o N Comment: BOHLK; METHOD 525; INST 204; 11/13/01; MDL "0 O CD CH Sorted via: Entry Number t CH O 0 o o Mo Name of Compound R Time Scani Mode Peak Area Pk Height O C 3 CD 3 chrysene d-12(IS) 22:40 1360 Auto 2,202,914 818,559 D

4 p-terphenyl d-14(IS) 20:50 1250 Auto 3,364,628 2,384,126 5 acenaphthene d-10(SURR 12:17 737 Auto 1,903,771 1,260,000 6 phenanthrene d-10(SURR 16:55 1015 Auto 3,147,793 1,289,898 7 chrysene d-12 (SURR) 22:40 1360 Auto 2,202,914 818,559 8 1,3-d imethy1-2-n itrobe 7:58 478 Auto 1,250,770 665,226 9 triphenyl phosphate (S 22:85 1325 Auto 1,699,053 706,721 10 perylene d-12 (SURR) 26:57 1617 Auto 1,329,424 241,598 11 hexachlorocyclopentad i 10:08 608 Auto 11,129 6,144 12 hexachlorobenzene 15:20 920 Auto 42,439 17,705 13 simazine 16:06 966 Auto 14,140 3,335 14 atrazine 16:16 976 Auto 19,774 5,782 15 alachlor 18:23 1103 Auto 46,224 24,398 16 b is(2-ethyIhexyl Jadipa 21:58 1318 Auto 61,566 11,597 17 b is (2-ethy Ihexy l phtha 22:58 1378 Auto 410,274 106,188 18 benzo(a pyrene 26:45 1605 Auto 70,994 7,263 19 eptc 10:33 633 Auto 842,011 523,945 20 2,6-d in itrotoluene 11:55 715 Auto 274,208 75,980 21 2,4-d in itrotoluene 12:55 775 Auto 233,689 60,736 22 molinate 13:02 782 Auto 372,673 193,721 23 terbac il 17:21 1041 Auto 220,510 74,257 24 acetochlor 18:12 1092 Auto 282,933 155,867 25 metribuzin 18:14 1094 Auto 20,620 7,735 26 metolachlor 19:08 1148 Auto 139,836 53,761 27 butachlor 20:23 1223 Auto 45,102 18,957 28 4,4'-dde 20:46 1246 Auto 191,122 121,623

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NYC-WTC_000029459 · Box DEP Box 20

Gas chromatography-mass spectrometry analysis results for sample AD25458 including Hexachlorobenzene and other compounds from November 2001.

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