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Method detection limit verification, sample AD25458, Nov 2001

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Laboratory analysis report verifying method detection limits for pesticides and organic compounds in sample AD25458 during November 2001.

NYC-WTC_000029500–000029504

Folder label: “525 X 10/29/01 AN 11/13 - 11/14/01

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o Io “0 C o Integration Report Quanfile: MDLA1113 Quan Entr ies: 28 O o o o N Comment: BOHLKi METHOD 525; INST 204; 11/13/01; NDL "0 O (O CH Sorted via: Entry Number 1 — O C 9 U No Name of Compound R Time Scani Node o Peak Area Pk Height o C 3 0 3 chrysene d-12(IS) 22:41 1361 Auto 2,393,467 881,296 4 p-terphenyl d-14(IS) 20:50 1250 Auto 3,465,162 2,101,019 5 acenaphthene d-10(SURR 12:17 737 Auto 2,132,503 1,112,637 6 phenanthrene d-10(SURR 16:55 1015 Auto 3,321,120 1,419,886 7 chrysene d-12 CSURR) 22:41 1361 Auto 2,393,467 881,296 8 1,3-d imethy1-2-n itrobe 7:58 478 Auto 1,373,513 768,372 9 triphenyl phosphate (8 22:06 1326 Auto 1,803,260 601,448 10 perylene d-12 CSURR) 26:57 1617 Auto 1,240,092 233,930 11 hexachlorocyclopentad i 10:09 609 Auto 14,809 7,475 12 hexach lorobenzene 15:20 920 Auto 56,070 22,889 13 simazine 16:05 965 Auto 15,452 4,559 14 atrazine 16:16 976 Auto 23,131 6,763 15 alachlor 18:23 1103 Auto 57,278 25,118 16 bis (2-ethy Ihexy Dadipa 21:59 1319 Auto 82,038 13,318 17 bis(2-ethyIhexyl)phtha 22:58 1378 Auto 771,840 212,523 18 benzo(a)pyrene 26:45 1605 Auto 72,477 7,274 19 eptc 10:33 633 Auto 924,180 603,526 20 2,6-d in itrotoluene 11:56 716 Auto 272,399 88,180 21 2,4-d in itrotoluene 12:55 775 Auto 262,189 74,554 22 molinate 13:03 783 Auto 396,153 184,442 23 terbacil 17:21 1041 Auto 213,855 76,094 24 acetochlor 18:12 1092 Auto 299,066 170,500 25 metribuzin 18:14 1094 Auto 34,045 13,008 26 metolachlor 19:09 1149 Auto 141,246 61,657 27 butachlor 20:23 1223 Auto 56,728 27,265 28 4,4'-dde 20:46 1246 Auto 236,871 176,590

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NYC-WTC_000029459 · Box DEP Box 20

Gas chromatography-mass spectrometry analysis results for sample AD25458 including Hexachlorobenzene and other compounds from November 2001.

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