Laboratory data sheet for samples AD24722-24723, Oct-Nov 2001

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1 o O C O O O Mass List File: C:\DFTB1107 Date: Nou-08-1991 04:35:26 CT o' O N Comment: BOHLKJ METHOD 525; INST 204; 11/07/01; DFTPP/ENDRIN U co O co Scan No: 1103 Retention Time: 18:23 RIC: 5313744 Mass Range: 47 - 444 — 9 (1 # Peaks: 173 Mass of Base Peak: 442 Int: 892819 Threshold: 0 % O o o C Mass Intensity X Base Mass Intensity % Base Mass Intensity % Base 3 CD

47 2,925 0.33 83 5,053 0.57 124 4,521 0.51 48 3,723 0.42 84 6,648 0.74 125 3,457 0.39 49 23,936 2.68 85 3,191 0.36 127 163,297 18.29 50 125,531 14.06 86 11,968 1.34 128 14,361 1.61 51 335,372 37.560 87 3,457 0.39 129 68,617 7.69 52 17,021 1.91 91 5,585 0.63 130 7,180 0.80 55 3,191 0.36 92 4,787 0.54 134 2,127 0.24 56 9,308 1.04 93 34,388 3.84 135 7,180 0.80 57 16,489 1.85 94 2,393 0.27 136 2,925 0.33 61 7,446 0.83 98 33,244 3.72 137 3,723 0.42 62 7,180 0.80 99 14,361 1.61 141 10,106 1.13 63 8,776 0.98 101 5,585 0.63 142 4,787 0.54 65 2,925 — 0.33 103 5,319 0.60 143 2,659 0.30 68 5,053 0.57 104 5,319 0.60 146 3,723 0.42 69 235,106 26.336 105 7,978 0.89 147 5,585 0.63 73 5,851 0.66 106 2,393 0.27 148 19,680 2.20 74 35,106 3.93 107 72,874 8.07 149 3,191 0.36 75 36,436 4.08 108 10,106 1.13 153 3,989 0.45 76 15,425 1.73 110 140,425 15.73 154 3,723 0.42 77 220,478 24.69 ill 14,361 1.61 155 7,978 0.89 78 14,627 1.64 116 3,191 0.36 156 8,776 0.98 79 32,180 3.60 117 96,276 10.78 157 2,659 0.30 80 16,223 1.82 118 7,712 0.86 158 2,659 0.30 81 11,702 1.31 122 6,382 0.71 159 2,659 0.30 82 3,723 0.42 123 6,648 0.74 160 4,255 0.48