Quality control analysis sample AD24488, November 2001

z Z oK O 3 o CD _s

1 U C O CT o Nass List File: C:\DFTB1103 Date: Nou-04-1991 03:36:07 o o' o N CO Comment: BOHLKi HETHOD 525J INST 204; 11/03/01; DFTPP O U Scan No: 1104 Retention Time: 18:24 RIC: 6285689 Nass Range: 47 - 444 — 9 CH # Peaks: 156 Nass of Base Peak: 442 Int: 1116319 Threshold: 0 % O o o C Nass Intensity X Base Nass Intensity X Base Nass Intensity X Base 2CD

47 4,861 0.44 84 6,250 0.56 128 17,013 1.52 49 24,305 2.18 / 85 8,680 0.78 129 83,333 7.46 50 132,291 11.85% 86 12,847 1.15 130 7,291 0.65 51 401,736 35.99 91 5,902 0.53 134 4,166 0.37 52 18,055 1.62 92 5,208 0.47 135 10,416 0.93 55 4,861 0.44 93 41,319 3.70 136 3,819 0.34 56 13,541 1.21 94 4,166 0.37 137 2,777 0.25 57 10,763 0.96 98 38,541 3.45 140 2,430 0.22 61 5,902 0.53 99 18,402 1.65 141 18,402 1.65 62 4,513 0.40 100 2,430 0.22 142 5,208 0.47 63 13,194 1.18 101 9,027 0.81 143 3,472 0.31 67 2,430 0.22 103 8,680 0.78 146 2,777 0.25 68 5,9022. 0.53 104 9,722 0.87 147 9,027 0.81 69 268,402 24.04 105 7,638 0.68 148 16,666 1.49 73 4,861 0.44 107 85,763 7.68 153 3,472 0.31 74 44,791 4.01 108 10,763 0.96 154 3,819 0.34 75 37,847 3.39 110 162,152 14.53 155 4,861 0.44 76 13,194 1.18 ill 19,444 1.74 156 9,722 0.87 77 267,361 23.95 117 113,541 10.17 160 3,125 0.28 78 15,625 1.40 118 7,638 0.68 161 6,944 0.62 79 29,166 2.61 122 9,027 0.81 165 5,208 0.47 80 17,013 1.52 123 6,597 0.59 166 6,250 0.56 81 19,791 1.77 124 3,125 0.28 167 28,819 2.58 82 4,513 B.40 125 4,513 0.40 /168 11,805 1.06 83 4,513 0.40 127 193,055 17.29, 172 3,819 0.34