Method detection limit verification, Oct 2001

2 Z X K O O CO

3 _s

o “0 C 1 o Mass List File: E:\DFTB1030 Date: Oct-31-1991 00:29:56 O O o o o Comment: BOHLK; METHOD 525; INST 204; 10/30/01; DFTPP/ENDRIN U N o 00 C Scan No: 1108 Retention Time: 18:28 RIC: 5034055 Mass Range: 47 - 444 — 9 (O CH # Peaks: 156 Mass of Base Peak: 442 lnt: 930376 Threshold: 0 % O o O C Nass Intensity % Base Mass Intensity A Base Mass Intensity % Base 3 0 13 185 8 j 064 0.87 228 2,956 0.32 321 2,419 0.26 186 59,139 6.36 229 4,032 0.43 323 15,322 1.65 187 13,172 1.42 234 2,419 0.26 324 4,032 0.43 188 2,956 0.32 240 1,612 0.17 328 2,419 0.26 189 3,763 0.40 244 33,333 3.58 334 11,021 1.18 192 3,494 0.38 245 5,376 0.58 335 5,913 0.64 196 9,139 0.98 246 9,677 1.04 346 3,225 0.35 198 485,483 52.18 255 328,225 35.28 352 5,107 0.55 199 29,569 3.18 256 38,172 4.10 353 4,301 0.46 203 3,225 0.35 258 15,591 1.68 354 10,483 1.13 204 12,096 1.30 259 2,956 0.32 365 38,440 4.13 205 19,892 2.14 265 5,376 0.58 366 5,376 0.58 206 85,483 9.19 273 11,021 1.18 372 7,526 0.81 207 13,978 1.50 274 37,096 3.99 373 4,032 0.43 208 4,032 0.43 275 164,784 17.71 383 2,419 0.26 211 3,225 0.35 276 23,118 2.48 402 4,032 0.43 216 3,494 0.38 277 12,365 1.33 403 5,645 0.61 217 22,849 2.46 278 3,763 0.40 421 4,569 0.49 218 3,225 0.35 293 5,107 0.55 422 7,258 0.78 221 7,526 0.81 296 32,258 3.47 423 44,354 4.77 222 3,494 0.38 297 6,989 0.75 424 10,215 1.10 223 4,838 0.52 303 5,645 0.61 441 113,709 12.22) 224 47,043 5.06 304 2,688 0.29 442 930,376 100.01 225 13,440 1.44 315 5,913 0.64 443 156,451 16.82 227 21,505 2.31 316 2,688 0.29 444 9,677 1.04