Method detection limit verification, Oct 2001

Z Z K - o o 3 CD _s

i o U C O o Mass List File: E:DFTB1030 Date: Oct-31-1991 00:29:56 CT o' O O Comment: BOHLK: METHOD 525; INST 204; 10/30/01; DFTPP/ENDRIN -0 N o CO C Scan No: 1108 Retention Time: 18:28 RIC: 5034055 Mass Range: 47 - 444 — (O # Peaks: 156 Mass of Base Peak: 442 Int: 930376 Threshold: 0 % 9 N U o o Mass Intensity A Base Mass Intensity % Base Mass Intensity % Base C 3 CD

47 5,107 0.55 85 3,763 0.40 127 168,279 18.09 49 15,322 1.65 86 8,602 0.92 128 13,172 1.42 50 101,881 10.95 / 87 2,956 0.32 129 69,086 7.43 51 316,666 34.041 91 6,451 0.69 130 7,526 0.81 52 12,096 1.30 92 4,301 0.46 131 1,881 0.20 55 3,494 0.38 93 34,139 3.67 134 2,956 0.32 56 6,182 0.66 98 31,451 3.38 135 6,720 0.72 57 14,247 1.53 99 12,903 1.39 136 2,956 0.32 61 5,107 0.55 101 6,182 0.66 137 3,494 0.38 62 4,032 0.43 103 5,107 0.55 141 12,365 1.33 63 8,333 0.90 104 6,720 0.72 142 4,569 0.49 68 0.52 105 4,032 0.43 147 5,107 0.55 69 200,537 21.55 106 2,688 0.29 148 14,516 1.56 73 3,763 L.80.40 107 74,731 8.03 153 3,763 0.40 74 37,903 4.07 108 9,677 1.04 154 2,956 0.32 75 34,139 3.67 110 115,322 12.40 155 6,182 0.66 76 10,752 1.16 ill 12,903 1.39 156 8,870 0.95 77 219,892 23.63 112 2,956 0.32 158 3,225 0.35 78 11,827 1.27 116 5,376 0.58 160 5,107 0.55 79 29,569 3.18 117 88,440 9.51 161 4,569 0.49 80 15,053 1.62 118 5,107 0.55 165 4,032 0.43 81 14,516 1.56 122 5,913 0.64 166 4,569 0.49 82 2,419 0.26 123 7,258 0.78 167 23,387 2.51 83 2,419 0.26 124 5,107 0.55 168 9,139 0.98 84 5,376 0.58 125 3,225 0.35 172 2,688 0.29