Quality control analyses log, Oct 2001

Z Z - - O o co 3 o _s

U 1 CD C O CD CD Mass List File: E:\DFTA1025 Date: Oct-25-1991 18:36:30 o' CD Comment: BOHLK: METHOD 525; INST 204; 10/25/01; DFTPP/ENDRIN U N o CO — N Scan No: 1111 Retention Time: 18:31 RIC: 6756526 Mass Range: 49 - 444 0 O) # Peaks: 167 Mass of Base Peak: 442 Int: 1272569 Threshold: 0 % U o o C Mass Intensity % Base Mass Intensity % Base Mass Intensity % Base 3 CD D 0) 197 198 5,208 636,111 0.41 T 244 39,236 7,638 3.08 0.60 323 324 25,694 5,208 2.02 0.41 199 39,930 11,111 0.87 327 5,902 0.46 203 4,166 0.33 247 3,472 0.27 328 4,166 0.33 204 13,888 1.09 254 5,208 0.41 334 14,930 1.17 205 26,388 2.07 255 404,861 31.81 335 4,861 0.38 206 110,416 8.68 256 52,083 4.09 346 4,513 0.35 207 14,930 1.17 257 5,555 0.44 352 4,166 0.33 208 3,819 0.30 258 21,527 1.69 353 5,555 0.44 210 2,430 0.19 259 3,472 0.27 354 12,847 1.01 211 4,513 0.35 265 8,333 0.65 365 52,083 4.09^ 215 3,472 0.27 266 3,125 0.25 366 9,722 0.76 217 24,652 1.94 273 12,500 0.98 372 18,402 1.45 221 9,027 0.71 274 50,347 3.96 / 373 6,250 0.49 222 3,472 0.27 275 214,236 16.83 383 3,819 0.30 223 6,597 0.52 276 29,166 2.29 402 6,250 0.49 224 61,805 4.86 277 22,222 1.75 403 9,027 0.71 225 21,180 1.66 293 5,555 0.44 421 8,680 0.68 227 29,513 2.32 296 52,083 4.09 422 5,208 0.41 228 5,208 0.41 297 7,638 0.60 423 64,583 5.08 / 229 6,250 0.49 303 6,944 0.55 424 15,625 1.23 235 4,166 0.33 313 2,083 0.16 441 161,805 12.71- 236 3,125 0.25 314 3,472 0.27 442 1,272,569 100.003 237 2,777 0.22 315 7,638 0.60 443 231,597 18.20), 243 4,513 0.35 316 6,250 0.49 444 18,402 1.45