Laboratory method data sheet for sample AD26887, Oct 2001

2 Z K K o o c 3 _s

1 o C O O Mass List File: E:\DFTA1024 Date: Oct-24-1991 20:15:08 CT o' O o Comment: BOHLK: METHOD 525; INST 204; 10/24/01; DFTPP U N o CO Scan No: 1111 Retention Time: 18:31 RIC: 7698230 Mass Range: 47 - 444 — 0 N <0 # Peaks: 160 Mass of Base Peak: 442 Int: 1256779 Threshold: 0 X U o o Mass Intens ity % Base Mass Intens ity X Base Mass Intensity % Base C 3 CD — 47 4,661 0.37 83 6,779 0.54 124 5,084 0.40 48 3,389 0.27 84 7,203 0.57 127 247,457 19.69 49 29,661 2.36 85 5,084 0.40 128 22,033 1.75 50 191,101 15.21 / 86 18,220 1.45 129 109,322 8.70 51 518,220 41.23? 91 6,355 0.51 130 11,016 0.88 52 22,033 1.75 92 4,661 0.37 134 5,084 0.40 55 6,355 0.51 93 55,932 4.45 135 8,898 0.71 56 16,949 1.35 94 5,084 0.40 136 3,813 0.30 57 16,525 1.31 98 51,694 4.11 141 15,254 1.21 61 8,474 0.67 99 19,915 1.58 142 7,627 0.61 62 7,627 0.61 101 9,745 0.78 143 9,322 0.74 63 11,016 0.88 103 9,745 0.78 146 4,661 0.37 65 4,237 0.34 / f 104 10,593 0.84 147 12,288 0.98 68 5,932 0.47/ (o 105 10,169 0.81 148 23,305 1.85 69 73 74 357,203 8,898 50,000 2.744 3.98 ’ 109 ? 07 ‘08 107,627 13,983 2,966 8.56 1.11 0.24 150 151 153 3,389 4,237 8,898 0.27 0.34 0.71 75 47,457 3.78 110 204,661 16.28 155 8,474 0.67 76 15,677 1.25 111 23,728 1.89 156 12,711 1.01 77 350,423 27.88 112 8,050 0.64 161 9,745 0.78 78 22,033 1.75 116 4,237 0.34 165 7,627 0.61 79 40,254 3.20 117 143,644 11.43 166 5,508 0.44 80 22,457 1.79 118 11,016 0.88 167 39,406 3.14 81 22,881 1.82 122 8,474 0.67 168 17,796 1.42 82 6,779 0.54 123 9,745 0.78 170 2,542 0.20