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GCMS analysis results for sample AE11423, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11423 conducted on May 30, 2002.

NYC-WTC_000025479–000025493

Folder label: “GCMS X 5/16/02 A 5/20/02

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Scanned page image, NYC-WTC_000025488
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052002\11423.D Vial: 13 Acq On : 20 May 2002 11:03 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Methylene Chloride Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.71 0.36 ug/L 274075 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methylene Chloride 84 CH2C12 000075-09-20 89 2 Methylene Chloride 84 CH2C12 000075-09-2-50 3 Methylene Chloride 84 CH2C12 000075-09-2 32 4 Methylene Chloride 84 CH2C12 000075-09-2 17

Z0 Abundance Scan 107 (3.708 min): 11423. D (-96) (-) m/z 43.10 100.00% 43 49

5000 84

■ 1 r i ‘ 1 11 i1■■ 'i 111 1 i 1 1 1 1 i 3740 3,40 3.60 3.80 4.00 01 0 44 _ 88 " r 1" i1' " i " '' r " 11" '11"1 I '11 i " " I"1 m/z 49.10 80.07% n/z-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #111041: Methylene Chloride 49 ""Mudayu 84 5000 • * > i ‘1 * * ।1 * ■ * "i 11 11111. । । 3.40 3.60 3.80 4.00 46 m/z 41.10 51.06% 2629 41 | ,52 59 65 73 77 88 Ol " 11'1'1111111111111111 ii ‘+| 11111111111!11111 1 1" i ‘ " 11" " i " ■ ■ r ' ■' i" " i "1 -HP n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111039: Methylene Chloride 49 84 M hmn 3.40 3.60 3.80 4.00 5000 m/z 84.00 48.30%

2831 3538 43 ol " i" " i ■ " ' i " " I " " r ■" i" " 111" I" 111' ,52 57 67 71 I 1'' i" " P11111"11" " 111 "I "1 77 88 — ‘ I’’’ MLwymun., Tl/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111040: Methylene Chloride ■ ' ■ i ■ ■ 1 ................. । । t 49 3.40 3,60 3.80 4.00 84 m/z 51.10 28.44%

5000 "MAAWpqput"Wtept-vAN 35

m/z-> 14 2528 32 38441 0 " i" TTHTT TTTTTTHTTP | 70 +2 T00011000—0300—0—71030111 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 88 j'1H i".. ।. 3.40 3.60 3.80 4.00

11423.D 050102.M Thu May 23 10:49:42 2002 Page 5

NYC-WTC_000025488

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NYC-WTC_000025488Source: NYC Law Department, mirrored locally

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