GCMS reference standard results for sample AE11417, May 2002

Quantitation Report (QT Reviewed) 2 z - K o o 2 CD Data File : C:\MSDCHEM\l\DATA\052002\516REF2.D Vial: 6 — Acq On : 20 May 2002 5:22 pm Operator: Mclean o Sample : 5/16 eh Inst Instrumen "0 C 1 O o o Mise : Multiplr: 1.00 o' o o N MS Integration Params: EVENTS.E "0 o CH C Quant Time: May 22 15:56 2002 Quant Results File: 050102.RES — 0 o o Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) o Q Title : 508 Modified GC/MS scan C 3 Last Update : Mon May 13 11:40:29 2002 CD Response via : Initial Calibration Abundance TIC: 516REF2.D 2600000- O y % o 2 2400000 2o V 76 2g g € s 2200000 $ z I 11 c £2 N

2000000 2o M g 5 e l § 1800000 9 i $ 1600000 li O

i 2 o 10 z5 CM

1400000 0 .» 2 2® 16 i 1 t 6s L s Co &< o ! 2 CI s ri8 c 3 £ | g 1200000 2 8a8 & 8 ! i 8

1 2 58 2 88 o a 9 2 | 1000000 88:8 &2 (4883 II - 63 18 29 9 28I 2 I L 5C

Ig 51 t £ 1 8 s 1 800000 29:8 I88 Q on-ge No— i 1s 8

I 2 2 a 2 I 2 2 18 I 92 5 8 600000 l k8 ai I m§ CM w in C o N

1 g8 ce 5 400000 I ? o ! S 8 p ! 200000

U — N — 0 — Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

516REF2.D 050102.M Wed May 22 15:56:41 2002 Page 3