GC/MS analysis results for sample AE11412, May 28 2002

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Data File : C:\MSDCHEM\1\DATA\051702\11411.D Vial: 20 Acq On : 18 May 2002 5:05 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.132 3 9 16 BV 5 3163 41098 ' 0.08% 0.014% 2 3.702 95 106 109 PV 8 3689 113370 0.22% 0.038% 3 3.732 109 111 116 W 6 4444 94007 0.18% 0.032% 4 3.773 116 118 122 W 4 4102 74988 0.14% 0.025% 5 3.814 122 125 129 W 4 3701 75640 0.15% 0.025%

6 4.172 180 186 198 W 10 2123 68129 0.13% 0.023% 7 4.272 198 203 206 PV 5 2340 34368 0.07% 0.012% 8 4.954 314 319 329 W 14898 257707 0.50% 0.087% 9 5.042 329 334 337 PV 6 3987 69824 0.13% 0.023% 10 5.071 337 339 343 W 4 2198 33310 0.06% 0.011%

11 5.424 394 399 403 W 4 3606 74322 0.14% 0.025% 12 5.559 415 422 426 PV 6 2313 53614 0.10% 0.018% 13 5.635 426 435 453 W 6 10686 298303 0.57% 0.100% 14 5.976 487 493 513 W 850823 14800764 28.46% 4.973% 15 6.099 513 514 534 W 8 4050 162331 0.31% 0.055%

16 6.669 606 611 614 PV 6 1360 15792 0.03% 0.005% 17 7.733 785 792 810 PV 2 8368 245374 0.47% 0.082% 18 9.313 1056 1061 1070 PV 4 1853 38873 0.07% 0.013% 19 9.936 1155 1167 1189 PV 1902677 36008518 69.24% 12.098% 20 12.404 1582 1587 1594 PV 2 3417 50189 0.10% 0.017%

21 13.432 1749 1762 1782 PV 2532224 48197641 92.68% 16.193% 22 13.579 1782 1787 1795 W 3 8409 151603 0.29% 0.051% 23 15.694 2139 2147 2160 W 4 1909 42904 0.08% 0.014% 24 16.746 2318 2326 2334 PV 3 4013 74208 0.14% 0.025% 25 17.145 2389 2394 2401 W 2 8562 140748 0.27% 0.047%

26 17.657 2475 2481 2497 PV 4 3968 63015 0.12% 0.021% 27 18.567 2621 2636 2658 BV 2638634 52001865 100.00% 17.471% 28 18.961 2686 2703 2707 BV 3 2042 39865 0.08% 0.013% 29 20.547 2959 2973 2985 PV 1347278 26377141 50.72% 8.862% 30 21.394 3096 3117 3126 PV 2 11567 187836 0.36% 0.063%

31 22.575 3312 3318 3331 W 2 18825 343661 0.66% 0.115% 32 22.956 3370 3383 3402 PV 2 2354145 49568290 95.32% 16.653% 33 23.109 3402 3409 3439 W 20106 596916 1.15% 0.201% 34 29.984 4572 4579 4587 PV 4 1995 46453 0.09% 0.016% 35 30.806 4700 4719 4742 BV 2 1719001 39100624 75.19% 13.137%

36 30.947 4742 4743 4746 W 2 8510 86681 0.17% 0.029% 37 30.971 4746 4747 4752 W 3 6701 122261 0.24% 0.041%

11411.D 050102.M Tue May 21 15:54:52 2002 Page 1

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