GCMS analysis results for sample AE11409, May 22 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\051702\11384.D Vial: 11 Acq On : 17 May 2002 8:56 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.696 94 105 108 PV 7 4945 137069 0.32% 0.057% 2 3.732 108 111 114 W 5 6123 109172 0.26% 0.045% 3 3.761 114 116 118 W 2 5570 84229 0.20% 0.035% 4 3.779 118 119 121 W 2 5778 49186 0.12% 0.020% 5 3.802 121 123 129 W 5 5189 124901 0.30% 0.052%

6 5.024 328 331 333 W 3 3547 36243 0.09% 0.015% 7 5.042 333 334 342 W 6 2911 60351 0.14% 0.025% 8 5.400 390 395 400 W 5 2630 51772 0.12% 0.022% 9 5.964 481 491 515 PV 577196 10963683 25.90% 4.565% 10 6.117. 515 517 519 W 2 2748 34641 0.08% 0.014%

11 7.739 788 793 814 PV 4 4885 175832 0.42% 0.073% 12 9.930 1156 1166 1187 PV 1464637 29234354 69.07% 12.171% 13 12.404 1579 1587 1596 W 20647 321814 0.76% 0.134% 14 13.426 1748 1761 1782 PV 2107394 39043712 92.24% 16.255% 15 13.585 1782 1788 1799 W 3 6228 127813 0.30% 0.053%

16 16.746 2316 2326 2339 W 2 3072 89393 0.21% 0.037% 17 17.145 2390 2394 2401 W 2 5831 93717 0.22% 0.039% 18 17.663 2463 2482 2486 PV 5 2901 58657 0.14% 0.024% 19 18.567 2625 2636 2659 PV 2244066 42328388 100.00% 17.623% 20 20.142 2900 2904 2912 W 4 1984 37879 0.09% 0.016%

21 20.542 2953 2972 2984 PV 1134863 21190820 50.06% 8.822% 22 21.394 3111 3117 3124 BV 4 7716 130714 0.31% 0.054% 23 22.580 3309 3319 3332 W 2 13553 261904 0.62% 0.109% 24 22.951 3372 3382 3401 PV 2 1917200 40414220 95.48% 16.826% 25 23.109 3401 3409 3426 W 2 14987 436108 1.03% 0.182%

26 25.089 3737 3746 3756 PV 2 1960 47641 0.11% 0.020% 27 26.505 3978 3987 3993 BV 2 3105 53803 0.13% 0.022% 28 30.800 4707 4718 4772 PV 2 1396674 32208782 76.09% 13.410% 29 31.123 4772 4773 4780 W 6 1137 22459 0.05% 0.009% 30 34.702 5371 5382 5440 PV 2 862586 22171179 52.38% 9.231%

31 35.054 5440 5442 5444 W 3 1370 14029 0.03% 0.006% 32 35.095 5444 5449 5458 W 8 1292 29865 0.07% 0.012% 33 35.172 5458 5462 5464 PV 2 992 12952 0.03% 0.005% 34 35.360 5485 5494 5495 PV 6 1092 21158 0.05% 0.009% 35 35.377 5495 5497 5501 W 3 1258 13339 0.03% 0.006%

11384.D 050102.M Tue May 21 11:56:05 2002 Page 1

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