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GCMS analysis results for sample AE11310, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE11310 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000025012–000025021

Folder label: “GCMS X 5/14/02 A 5/21/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY21O2\113O9.D Vial: 23 Acq On : 21 May 2002 10:27 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 22 9:12 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 22 09:03:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.57 178 240 N.D. 36) Di-n-butylphthalate 27.50 149 38561 1.14 ug/1 # 99 37) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.57 228 1227 N.D. 42) Bis(2-ethylhexyl) phthalate 33.80 149 812 N.D. 43) Chrysene 33.57 228 1227 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 4 6) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.78 252 1268 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 11309.D GCMS0520.M Wed May 22 09:13:10 2002 Page 2

NYC-WTC_000025015

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NYC-WTC_000025015Source: NYC Law Department, mirrored locally

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