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GCMS analysis results for sample AE10245, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10245 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024863–000024870

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020509\10245.D Vial: 23 Acq On : 10 May 2002 8:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.152 518 523 569 rBV 375147 867892 19.71% 3.650% 2 11.370 1399 1411 1433 rBV 1185608 3150074 71.54% 13.249% 3 16.534 2274 2290 2311 rBV 1500891 3965030 90.05% 16.676% 4 24.460 3619 3639 3655 rBV2 1469160 4103491 93.20% 17.259% 5 27.533 4146 4162 4176 rBV3 164834 453020 10.29% 1.905%

6 31.094 4755 4768 4778 rVB5 10499 33184 0.75% 0.140% 7 31.717 4854 4874 4894 rBV2 1447833 4403015 100.00% 18.519% 8 31.964 4908 4916 4928 rVB4 13185 40590 0.92% 0.171% 9 39.931 6258 6272 6291 rBV2 2013981 3881743 88.16% 16.326% 10 43.151 6809 6820 6850 rBV 1422149 2878159 65.37% 12.105%

Sum of corrected areas: 23776198

10245.D SCTVN02 0507 . M Tue May 14 14:26:32 2002 Page 1

NYC-WTC_000024865

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NYC-WTC_000024865Source: NYC Law Department, mirrored locally

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