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GCMS analysis report sample AE10245, May 2002

Machine-extracted title · confidence 80%

GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.

NYC-WTC_000024851–000024862

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020516\10245.D Vial: 21 Acq On : 17 May 2002 5:06 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.158 517 524 560 rBV 528885 1081107 37.75% 6.312% 2 11.376 1401 1412 1432 rBV 825163 2077776 72.55% 12.130% 3 15.453 2098 2106 2115 rVB3 5782 14699 0.51% 0.086% 4 16.534 2275 2290 2303 rBV 995017 2573937 89.88% 15.027% 5 24.455 3619 3638 3653 rBV 943405 2666905 93.12% 15.570%

6 27.551 4144 4165 4176 rBV2 595582 1701760 59.42% 9.935% 7 31.106 4758 4770 4778 rVB4 4980 16697 0.58% 0.097% 8 31.717 4856 4874 4897 rBV3 929493 2863897 100.00% 16.720% 9 31.952 4906 4914 4928 rVB4 7416 23796 0.83% 0.139% 10 38.538 6028 6035 6041 rBV3 13390 26249 0.92% 0.153% 11 39.931 6261 6272 6298 rBV2 1303303 2440322 85.21% 14.247% 12 43.151 6807 6820 6839 rBV 800696 1641621 57.32% 9.584%

Sum of corrected areas: 17128766

10245.D SCAN020507.M Fri May 17 10:46:25 2002 Page 1

NYC-WTC_000024855

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NYC-WTC_000024855Source: NYC Law Department, mirrored locally

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