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GCMS analysis results for sample AE10891, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10891 conducted on May 21, 2002, including surrogate recovery data.

NYC-WTC_000024242–000024253

Folder label: “GCMS X 5/10/02 A 5/15/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\MAY1502\10891.D Vial: 9 Acq On : 15 May 2002 9:54 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.014 211 215 224 rBV 62033 125405 3.87% 0.652% 2 7.793 295 300 319 rVB 39395 93779 2.90% 0.487% 3 8.141 334 338 370 rBV 725197 1603720 49.53% 8.336% 4 9.937 526 534 542 rBV2 14025 44616 1.38% 0.232% 5 12.164 771 777 794 rBV 1045046 2485688 76.78% 12.920% 6 15.792 1167 1173 1190 rBV 1584064 3237571 100.00% 16.828% 7 21.098 1745 1752 1769 rBV 1546767 3199304 98.82% 16.629% 8 23.242 1977 1986 1991 rBV 746469 1522277 47.02% 7.912% 9 25.542 2230 2237 2249 rBV2 1407747 3026750 93.49% 15.732% 10 33.606 3110 3117 3132 rBV2 1011994 2242825 69.27% 11.658% 11 37.831 3570 3578 3596 rBV2 555262 1657010 51.18% 8.613%

Sum of corrected areas: 19238945 10891.D GCMS0510.M Fri May 17 10:17:28 2002

NYC-WTC_000024247

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NYC-WTC_000024247Source: NYC Law Department, mirrored locally

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