GCMS analysis comments for sample AE10205, May 21 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\051602\10205.D Vial: 6 Acq On : 16 May 2002 6:36 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.731 94 111 117 PV 9 4472 209562 0.46% 0.081% 2 3.784 117 120 125 W 6 4184 97171 0.21% 0.037% 3 3.825 125 127 134 W 7 3505 106036 0.23% 0.041% 4 3.878 134 136 144 W 5 3764 96690 0.21% 0.037% 5 4.248 191 199 204 W 8 2564 66516 0.15% 0.026%

6 4.331 207 213 217 W 3 7470 125930 0.28% 0.049% 7 5.024 328 331 337 PV 4 4289 83290 0.18% 0.032% 8 5.071 337 339 345 W 5 1966 31174 0.07% 0.012% 9 5.406 386 396 403 PV 3 5431 122154 0.27% 0.047% 10 5.600 426 429 432 W 5 1718 26167 0.06% 0.010%

11 5.970 484 492 521 W 727450 13071745 28.82% 5.037% 12 7.733 781 792 813 PV 2 7634 220855 0.49% 0.085% 13 8.743 955 964 971 PV 5 1750 36848 0.08% 0.014% 14 9.936 1156 1167 1189 W 1655111 31634164 69.73% 12.190% 15 10.200 1206 1212 1219 PV 7 2246 39578 0.09% 0.015%

16 13.432 1747 1762 1780 PV 2253792 42330433 93.31% 16.311% 17 13.585 1780 1788 1797 W 7585 161307 0.36% 0.062% 18 15.700 2143 2148 2161 W 7 1767 39651 0.09% 0.015% 19 16.752 2316 2327 2335 PV 3 3094 69216 0.15% 0.027% 20 17.151 2389 2395 2402 W 4 6427 103303 0.23% 0.040%

21 17.662 2478 2482 2493 W 4 3136 54392 0.12% 0.021% 22 18.567 2624 2636 2648 PV 2352693 45364281 100.00% 17.480% 23 18.649 2648 2650 2661 W 3 3333 75113 0.17% 0.029% 24 20.541 2951 2972 2987 W 1209377 22814469 50.29% 8.791% 25 21.393 3111 3117 3126 W 3 9261 156724 0.35% 0.060%

26 22.580 3310 3319 3329 BV 15590 285765 0.63% 0.110% 27 22.950 3368 3382 3403 BV 2 2100958 43227670 95.29% 16.657% 28 23.109 3403 3409 3416 W 2 14901 356457 0.79% 0.137% 29 23.156 3416 3417 3423 W 3 2245 31522 0.07% 0.012% 30 30.806 4705 4719 4762 PV 2 1517472 34671189 76.43% 13.360%

31 31.070 4762 4764 4766 W 2 2940 38910 0.09% 0.015% 32 31.376 4812 4816 4826 W 4 4673 94913 0.21% 0.037% 33 33.838 5230 5235 5243 W 5 2687 50118 0.11% 0.019% 34 34.702 5371 5382 5410 PV 2 979547 23267482 51.29% 8.966% 35 34.872 5410 5411 5422 W 7 7629 213074 0.47% 0.082%

36 34.942 5422 5423 5432 W 5 3178 69439 0.15% 0.027% 37 35.348 5487 5492 5500 W 7 1801 50107 0.11% 0.019%

10205.D 050102.M Fri May 17 15:01:27 2002 Page 1

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