GCMS analysis results for sample AE10897, May 21 2002

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Laboratory report detailing GCMS analysis of sample AE10897 conducted on May 21, 2002, including surrogate recovery data.

NYC-WTC_000024100–000024112

Folder label: “GCMS X 5/10/02 A 5/16/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051602\10897.D Vial: 10 Acq On : 16 May 2002 9:52 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.532 74 77 81 PV 5 1818 27815 ' 0.07% 0.012% 2 3.690 96 104 105 PV 4 3583 56432 0.13% 0.024% 3 3.708 105 107 111 W 4 4274 82734 0.20% 0.035% 4 3.755 111 115 128 W 9 4036 203924 0.48% 0.086% 5 4.243 194 198 205 W 5 1803 35820 0.08% 0.015%

6 5.030 327 332 336 PV 7 3125 63625 0.15% 0.027% 7 5.065 336 338 340 W 2 2236 21096 0.05% 0.009% 8 5.412 388 397 402 PV 4 2705 42111 0.10% 0.018% 9 5.970 478 492 519 PV 573737 10712733 25.26% 4.520% 10 7.739 781 793 810 PV 3 5599 171020 0.40% 0.072%

11 8.743 957 964 975 W 3 5018 111973 0.26% 0.047% 12 9.936 1154 1167 1186 PV 1502951 29307657 69.11% 12.367% 13 12.410 1581 1588 1603 PV 3 1784 34398 0.08% 0.015% 14 13.432 1751 1762 1782 PV 2127936 39445008 93.01% 16.644% 15 13.585 1782 1788 1798 W 2 6596 127550 0.30% 0.054%

16 16.740 2318 2325 2338 PV 5 3136 70421 0.17% 0.030% 17 17.151 2379 2395 2402 BV 3 6323 112513 0.27% 0.047% 18 17.662 2468 2482 2486 BV 5 2620 43232 0.10% 0.018% 19 18.567 2624 2636 2661 PV 2228229 42410155 100.00% 17.895% 20 20.541 2960 2972 2986 PV 1183428 21806070 51.42% 9.201%

21 21.393 3112 3117 3124 PV 4 8831 137857 0.33% 0.058% 22 22.580 3312 3319 3330 PV 2 13479 254139 0.60% 0.107% 23 22.950 3369 3382 3403 PV 2 1934593 39732262 93.69% 16.765% 24 23.103 3403 3408 3421 W 3 14424 359996 0.85% 0.152% 25 26.505 3981 3987 3994 W 4 2876 60864 0.14% 0.026%

26 30.800 4704 4718 4760 PV 2 1336899 30576703 72.10% 12.902% 27 31.059 4760 4762 4778 W 6 3318 104538 0.25% 0.044% 28 31.376 4806 4816 4832 PV 3 15625 378914 0.89% 0.160% 29 34.702 5366 5382 5422 BV 845222 20438152 48.19% 8.624% 30 34.943 5422 5423 5425 W 2 2694 28261 0.07% 0.012%

31 34.966 5425 5427 5435 W 5 2018 32586 0.08% 0.014%

Sum of corrected areas: 236990560

10897.D 050102.M Fri May 17 15:05:30 2002 Page 1

NYC-WTC_000024105

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