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GCMS analysis with surrogate recovery, sample AE10895, May 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of sample AE10895 with 91% surrogate recovery for 2,4-DDD, conducted May 21, 2002.

NYC-WTC_000024070–000024082

Folder label: “GCMS X 5/10/02 A 5/16/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C: \MSDCHEM\1\DATA\051602\10895.D Vial: 8 Acq On : 16 May 2002 8:14 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.667 92 100 102 PV 7 2588 33220 0.08% 0.015% 2 3.725 102 110 113 W 7 3886 120847 0.31% 0.055% 3 3.749 113 114 116 W 2 3459 31478 0.08% 0.014% 4 3.773 116 118 123 W 5 2135 42574 0.11% 0.019% 5 3.814 123 125 126 W 2 1692 12939 0.03% 0.006%

6 3.831 126 128 132 W 4 2186 24343 0.06% 0.011% 7 4.237 193 197 202 W 3 2122 31427 0.08% 0.014% 8 4.783 285 290 294 PV 6 1890 29594 0.08% 0.013% 9 4.936 312 316 326 W 7 4287 84409 0.22% 0.038% 10 5.024 326 331 343 W 7 5341 154197 0.39% 0.070%

11 5.400 391 395 406 PV 6 3031 78564 0.20% 0.036% 12 5.629 428 434 448 W 10 3102 87244 0.22% 0.040% 13 5.970 485 492 523 PV 612620 11070111 28.25% 5.030% 14 7.739 787 793 802 BV 5 5208 111464 0.28% 0.051% 15 8.743 957 964 973 PV 2 5590 108468 0.28% 0.049%

16 9.936 1157 1167 1187 PV 1406227 27034176 68.99% 12.284% 17 13.426 1750 1761 1777 BV 1971823 36213763 92.41% 16.455% 18 13.526 1777 1778 1782 W 3 2539 33137 0.08% 0.015% 19 13.579 1782 1787 1798 W 2 5584 118848 0.30% 0.054% 20 16.746 2322 2326 2332 PV 3 2942 43792 0.11% 0.020%

21 17.151 2390 2395 2401 W 4 5821 98244 0.25% 0.045% 22 17.662 2474 2482 2490 W 4 3133 55309 0.14% 0.025% 23 18.567 2624 2636 2667 BV 2061683 39188147 100.00% 17.806% 24 20.541 2960 2972 2987 PV 2 1134284 21051953 53.72% 9.566% 25 21.393 3110 3117 3126 W 3 7987 142407 0.36% 0.065%

26 22.580 3309 3319 3327 PV 13143 241496 0.62% 0.110% 27 22.950 3367 3382 3403 PV 2 1790929 36445437 93.00% 16.560% 28 23.109 3403 3409 3426 W 3 13836 368416 0.94% 0.167% 29 30.800 4706 4718 4759 PV 2 1230619 27910107 71.22% 12.682% 30 31.047 4759 4760 4776 W 9 2545 111802 0.29% 0.051%

31 31.376 4806 4816 4838 PV 3 16270 373773 0.95% 0.170% 32 34.702 5371 5382 5403 PV 2 746080 18181047 46.39% 8.261% 33 34.831 5403 5404 5430 W 7 12181 445327 1.14% 0.202%

Sum of corrected areas: 220078060

10895.D 050102.M Fri May 17 15:03:43 2002 Page 1

NYC-WTC_000024075

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NYC-WTC_000024075Source: NYC Law Department, mirrored locally

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