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GC/MS results for unknown compounds and surrogates, sample AE10984, May

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS analysis of sample AE10984 with surrogate recovery data for 2,4-DDD.

NYC-WTC_000023991–000024013

Folder label: “GCMS X 5/10/02 A 5/14/02

Page image
Scanned page image, NYC-WTC_000023996
OCR text

OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\051402\10984.D Vial: 13 Acq On : 14 May 2002 11:17 pm Operator: Mclean Sample : 5/10 kb Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.132 3 9 24 BV 3 5308 129656 • 0.21% 0.035% 2 3.355 39 47 53 BV 10991 167621 0.27% 0.045% 3 3.408 53 56 63 W 6 3078 61334 0.10% 0.016% 4 3.555 77 81 85 PV 6 3330 52235 0.08% 0.014% 5 3.631 89 94 100 W 21236 352697 0.57% 0.094%

6 3.684 100 103 108 W 5 4865 103669 0.17% 0.028% 7 3.755 108 115 124 W 2 9963 352158 0.57% 0.094% 8 3.814 124 125 130 W 5 4168 73848 0.12% 0.020% 9 4.178 183 187 192 W 5 4695 94407 0.15% 0.025% 10 4.278 198 204 208 W 5 4226 85897 0.14% 0.023%

11 4.595 251 258 266 W 9 1886 56594 0.09% 0.015% 12 4.959 316 320 326 W 6 2810 47055 0.08% 0.013% 13 5.036 326 333 341 W 4 6580 158208 0.26% 0.042% 14 5.112 341 346 355 W 6 8724 193331 0.31% 0.052% 15 5.347 381 386 395 PV 8 1759 53642 0.09% 0.014%

16 5.424 395 399 413 W 6 3855 109627 0.18% 0.029% 17 5.535 413 418 424 W 6 2903 82804 0.13% 0.022% 18 5.582 424 426 428 W 2 2670 32050 0.05% 0.009% 19 5.659 435 439 448 W 7 3869 95440 0.16% 0.026% 20 5.982 485 494 515 W 1161313 20532252 33.40% 5.486%

21 6.111 515 516 523 W 6 3715 76494 0.12% 0.020% 22 7.016 664 670 680 W 7 .1985 71959 0.12% 0.019% 23 7.286 709 716 722 W 6 1925 38020 0.06% 0.010% 24 7.721 785 790 802 PV 18374 448707 0.73% 0.120% 25 7.797 802 803 807 W 3 2693 36619 0.06% 0.010%

26 8.120 849 858 860 W 5 1984 44355 0.07% 0.012% 27 8.379 899 902 912 W 7 1686 34704 0.06% 0.009% 28 8.749 959 965 972 W 2 9857 183824 0.30% 0.049% 29 8.814 972 976 988 W 7 3350 85605 0.14% 0.023% 30 9.031 1007 1013 1014 W 5 2015 29760 0.05% 0.008%

31 9.055 1014 1017 1023 W 5 2413 49997 0.08% 0.013% 32 9.254 1045 1051 1055 PV 8 2766 53488 0.09% 0.014% 33 9.301 1055 1059 1069 W 7 3997 100999 0.16% 0.027% 34 9.625 1107 1114 1116 PV 5 1703 28733 0.05% 0.008% 35 9.701 1122 1127 1131 W 5 2377 39715 0.06% 0.011%

36 9.936 1157 1167 1182 W 2237732 41902270 68.17% 11.197% 37 10.030 1182 1183 1193 W 6 2388 60935 0.10% 0.016%

10984.D 050102.M Thu May 16 14:41:27 2002 Page 1

NYC-WTC_000023996

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NYC-WTC_000023996Source: NYC Law Department, mirrored locally

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