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GC/MS results for unknown compounds and surrogates, sample AE10983, May

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS analysis of sample AE10983 with surrogate recovery data for 2,4-DDD.

NYC-WTC_000023949–000023969

Folder label: “GCMS X 5/10/02 A 5/14/02

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Scanned page image, NYC-WTC_000023954
OCR text

OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document E

Data File : C:\MSDCHEM\l\DATA\051402\10983.D Vial: 12 Acq On : 14 May 2002 10:28 pm Operator: Mclean Sample : 5/10 kb Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.132 3 9 18 BV 3 4959 102004 • 0.18% 0.030% 2 3.355 37 47 52 PV 2 13129 222423 0.40% 0.066% 3 3.402 52 55 60 W 6 4249 68092 0.12% 0.020% 4 3.567 73 83 89 PV 10 2762 87914 0.16% 0.026% 5 3.631 89 94 99 PV 26851 426674 0.77% 0.126%

6 3.731 99 111 112 W 6 7527 270190 0.49% 0.080% 7 3.755 112 115 129 W 3 11240 382695 0.69% 0.113% 8 4.013 150 159 163 W 8 4489 151109 0.27% 0.045% 9 4.172 183 186 192 W 6 5054 112755 0.20% 0.033% 10 4.272 196 203 210 W 4 4865 126159 0.23% 0.037%

11 5.036 327 333 341 W 6 5458 131769 0.24% 0.039% 12 5.106 341 345 364 W 7 8536 185992 0.33% 0.055% 13 5.353 382 387 394 PV 6 1653 38833 0.07% 0.012% 14 5.429 394 400 405 W 4 4849 82617 0.15% 0.024% 15 5.541 414 419 426 W 10 2309 72642 0.13% 0.022%

16 5.664 436 440 447 W 7 4210 78381 0.14% 0.023% 17 5.982 474 494 522 W 1101582 19762390 35.51% 5.853% 18 6.710 615 618 624 W 7 2193 49122 0.09% 0.015% 19 6.939 655 657 659 PV 3 1895 16728 0.03% 0.005% 20 7.010 664 669 673 W 4 2487 47747 0.09% 0.014%

21 7.286 708 716 726 W 10 2498 77129 0.14% 0.023% 22 7.451 736 744 749 W 8 3688 82589 0.15% 0.024% 23 7.721 786 790 810 W 2 16756 484338 0.87% 0.143% 24 8.109 853 856 860 W 5 3187 58493 0.11% 0.017% 25 8.367 891 900 912 W 3 7084 180718 0.32% 0.054%

26 8.749 958 965 972 W 2 9296 203785 0.37% 0.060% 27 8.814 972 976 989 W 6 5918 157295 0.28% 0.047% 28 9.025 1005 1012 1014 W 6 2336 43484 0.08% 0.013% 29 9.049 1014 1016 1018 W 3 2740 31997 0.06% 0.009% 30 9.254 1047 1051 1055 W 5 2684 49079 0.09% 0.015%

31 9.301 1055 1059 1071 W 5 4527 128162 0.23% 0.038% 32 9.695 1118 1126 1132 W 8 2395 77736 0.14% 0.023% 33 9.742 1132 1134 1138 W 5 2559 38830 0.07% 0.011% 34 9.936 1157 1167 1185 W 2055060 38605647 69.38% 11.433% 35 10.382 1238 1243 1257 W 6 6848 187375 0.34% 0.055%

36 10.612 1277 1282 1288 W 5 2161 38186 0.07% 0.011% 37 11.863 1485 1495 1504 PV 5 4101 77430 0.14% 0.023%

10983.D 050102.M Thu May 16 14:39:32 2002 Page 1

NYC-WTC_000023954

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NYC-WTC_000023954Source: NYC Law Department, mirrored locally

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