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GC/MS results for unknown compounds and surrogates, sample AE10982, May

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS analysis of sample AE10982 with surrogate recovery data for 2,4-DDD.

NYC-WTC_000023925–000023948

Folder label: “GCMS X 5/10/02 A 5/14/02

Page image
Scanned page image, NYC-WTC_000023930
OCR text

OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\051402\10982.D Vial: 11 Acq On : 14 May 2002 9:39 pm Operator: Mclean Sample : 5/10 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.126 3 8 15 BV 4 3979 85479 0.16% 0.026% 2 3.332 37 43 49 PV 15990 224338 0.42% 0.069% 3 3.543 72 79 83 PV 5 1805 25159 0.05% 0.008% 4 3.620 87 92 100 W 23857 417313 0.77% 0.128% 5 3.749 100 114 120 W 2 12444 394068 0.73% 0.120%

6 3.790 120 121 131 W 9 3905 144659 0.27% 0.044% 7 4.178 176 187 191 W 7 3743 109402 0.20% 0.033% 8 4.260 197 201 205 W 6 3459 72913 0.14% 0.022% 9 4.953 315 319 328 PV 5 2857 35634 0.07% 0.011% 10 5.036 328 333 338 W 4 4716 96692 0.18% 0.030%

11 5.100 338 344 353 W 6 8138 200632 0.37% 0.061% 12 5.341 382 385 389 PV 4 2053 27407 0.05% 0.008% 13 5.418 392 398 414 W 4 4292 97727 0.18% 0.030% 14 5.535 414 418 424 PV 6 2330 51778 0.10% 0.016% 15 5.653 433 438 447 W 6 4957 115208 0.21% 0.035%

16 5.976 485 493 521 W 1005561 17787611 32.94% 5.437% 17 6.176 521 527 532 W 9 2293 52682 0.10% 0.016% 18 7.016 667 670 673 W 5 2116 30878 0.06% 0.009% 19 7.286 711 716 726 W 9 1976 41654 0.08% 0.013% 20 7.727 783 791 808 PV 3 14380 419972 0.78% 0.128%

21 8.109 853 856 861 W 3 1948 33214 0.06% 0.010% 22 8.367 894 900 914 PV 6 6694 138405 0.26% 0.042% 23 8.749 954 965 973 BV 2 7933 155384 0.29% 0.047% 24 8.820 973 977 985 W 7 2224 47647 0.09% 0.015% 25 9.043 1004 1015 1021 PV 8 2206 66517 0.12% 0.020%

26 9.254 1044 1051 1056 W 5 2462 57606 0.11% 0.018% 27 9.313 1056 1061 1075 W 5 3477 104897 0.19% 0.032% 28 9.936 1157 1167 1185 PV 1975154 36963766 68.44% 11.299% 29 10.259 1215 1222 1225 PV 6 1397 17947 0.03% 0.005% 30 11.869 1490 1496 1502 W 5 1799 28420 0.05% 0.009%

31 12.039 1520 1525 1531 W 2 3634 68730 0.13% 0.021% 32 12.715 1636 1640 1648 PV 4 1706 41510 0.08% 0.013% 33 13.432 1749 1762 1779 W 2629236 49742324 92.10% 15.205% 34 13.585 1779 1788 1797 W 8675 192521 0.36% 0.059% 35 13.831 1821 1830 1834 W 5 2153 45796 0.08% 0.014%

36 14.254 1896 1902 1908 PV 4 2253 41166 0.08% 0.013% 37 15.700 2140 2148 2155 W 5 2140 46560 0.09% 0.014%

10982.D 050102.M Thu May 16 14:37:58 2002 Page 1

NYC-WTC_000023930

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NYC-WTC_000023930Source: NYC Law Department, mirrored locally

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