GCMS calibration verification for sample AE10901, May 2002

2 2 Quantitation Report (QT Reviewed) - K o o 2 Data File : C:\MSDCHEM\1\DATA\051402\510REF2.D Acq On : 14 May 2002 4:45 pm Vial: 5 Operator: Mclean co — o U I Sample : 5/10kb Inst : Instrumen C o O o Mise o Multiplr: 1.00 o' o N CD MS Integration Params: EVENTS.E "0 o 00 Quant Time: May 16 14:44 2002 Quant Results File: 050102.RES 0 o O Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) o Q C Title : 508 Modified GC/MS scan 3 Last Update : Thu May 16 14:34:28 2002 CD 3 Response via : Initial Calibration Abundance TIC: 510REF2.D O

2400000 g § Is 2200000 1 z o

3 c

5 n2 2000000 C

8 t z CM St 8 a 1800000 e $ g 1600000 Q S | 5- D 2o 8as 2 84 1400000 4 « 8 6 $ 8- o t o g4 ii 2 8 II 11 CO 3 @ 6e i§. I I Cl 1200000 8 g E8fg: 5 2 2 U. 2 18 gh 1 0 88 ! 0

1000000- s giy |e I5 69 82 5 i I lil O 2to 28 o2 800000 14898 2 &8 25 2. 3 E g Is fg 3« I 1 i a e f ! x

s g 8 Ig 8 2 O

11 0

600000

f f 2 86 Ng O

of to Ia th 8to £ ! 8 11 E 5§ 400000 £ & I $ ji 200000 I c a

A C

Time-> 0- - P.

4.00 t. . . V.

6.00 TTTd/-0T1d 8.00 10.00 k 12.00 - 14.00 16.00 18.00 20.00 — 22.00 24.00 26.00 28.00 30.00 —,'U 32.00 34.00 MA r— 36.00 r । 38.00 । i -1 ( )

510REF2.D 050102.M Thu May 16 14:44:26 2002 Page 3