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GCMS instrument log for sample AE09673, May 2002

Machine-extracted title · confidence 95%

Instrument log and analysis summary for GCMS testing of sample AE09673 conducted on May 23, 2002.

NYC-WTC_000023768–000023777

Folder label: “GCMS X 5/9/02 A 5/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY2002\9673.D Vial: 11 Acq On : 20 May 2002 5:01 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 2111:272002 iQuant Results File: G S0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.14 152 333900 40.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 1321402 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.08 164 623766 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.52 188 807815 40.00 ug/1 -0.01 38) Chrysene-dl2 33.58 240 412410 40.00 ug/1 -0.03 44) Perylene-dl2 37.78 264 243325 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.22 209 127587 40.70 ug/L 0.00 Spiked Amount 40.000 Recovery = 101.75% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.84 128 175 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.57 149 189 N.D. 26) 4-Chlorophenylphenylether 23.21 204 435 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.22 168 119 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.51 178 181 N.D. (#) = qualifier out of range (m) = manual integration 9673.D GCMS0520.M Tue May 21 11:28:17 2002 Page 1

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