GC/MS reference analysis results, sample AE09676, May 20-21 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY2002\REFl.D Vial: 7 Acq On : 20 May 2002 1:05 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 20 15:20 2002 <Quant Results File: GCMS0520.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.14 152 334131 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 1330238 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.08 164 630088 40.00 ug/1 0.00 3 0) Phenanthrene-dl0 25.52 188 849978 40.00 ug/1 -0.02 38) Chrysene-dl2 33.58 240 471203 40.00 ug/1 -0.02 44) Perylene-dl2 37.79 264 287170 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.23 209 125451 39.61 ug/L 0.00 Spiked Amount 40.000 Recovery 99.02%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.80 74 126082 12.57 ug/1 92 3) bis(2-Chloroethyl)ether 11.54 93 230924 17.38 ug/1 99 4) 1,3-Dichlorobenzene 12.04 146 165158 15.36 ug/1 97 5) 1,4-Dichlorobenzene 12.18 146 173570m 14.73 ug/1 6) 1,2-Dichlorobenzene 12.70 146 169756 16.63 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.03 45 566765 18.85 ug/1 97 8) N-Nitrosodi-n-propylamine 13.41 70 176842 18.74 ug/1 93 9) Hexachloroethane 13.55 117 62578 12.44 ug/1 # 84 11) Nitrobenzene 13.83 77 213527 18.47 ug/1 95 12) Isophorone 14.47 82 470455 20.55 ug/1 99 13) bis(2-Chloroethoxy)methane 15.15 93 280015 18.25 ug/1 100 14) 1,2,4-Trichlorobenzene 15.67 180 130957 15.76 ug/1 98 15) Naphthalene 15.83 128 566357 18.86 ug/1 99 16) Hexachlorobutadiene 16.38 225 55861 13.89 ug/1 99 18) Hexachlorocyclopentadiene 18.57 237 11592 4.54 ug/1 99 19) 2-Chloronaphthalene 19.33 162 279000 19.87 ug/1 96 20) Dimethylphthalate 20.43 163 333220 18.85 ug/1 100 21) 2,6-Dinitrotoluene 20.64 165 64650 17.57 ug/1 # 88 22) Acenaphthylene 20.61 152 431853 16.78 ug/1 99 23) Ac enapht hene 21.17 153 299814 19.50 ug/1 99 24) 2,4-Dinitrotoluene 21.82 165 76067 18.86 ug/1 93 25) Diethylphthalate 22.57 149 339719 20.80 ug/1 98 26) 4-Chlorophenylphenylether 22.71 204 148012 18.13 ug/1 98 27) Fluorene 22.70 166 303893 19.50 ug/1 99 29) Azobenzene 23.18 77 411588 17.49 ug/L 94 31) N-Nitrosodiphenylamine 23.11 168 95198 17.00 ug/1 # 90 32) 4-Bromophenylphenylether 24.18 248 79280 17.87 ug/1 97 33) Hexachlorobenzene 24.62 284 90020 18.91 ug/1 96 3 4) Phenanthrene 25.58 178 390965 19.07 ug/1 99

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0520.M Mon May 20 15:21:49 2002 Page 1

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