GC/MS reference analysis results, sample AE09683, May 15 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY1002\REFl.D Vial: 4 Acq On : 10 May 2002 3:59 pm Operator : Sample : GC/MS SCAN 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 13 9:05 2002 1Quant Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 13 08:58:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.17 152 562764 40.00 ug/1 -0.03 10) Naphthalene-d8 15.79 136 2058709 40.00 ug/1 -0.04 17) Acenaphthene-diO 21.11 164 1128850 40.00 ug/1 -0.03 3 0) Phenanthrene-dl0 25.55 188 1521387 40.00 ug/1 -0.02 38) Chrysene-dl2 33.62 240 828483m 40.00 ug/1 -0.02 44) Perylene-dl2 37.84 264 526337 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.25 209 170847 30.43 ug/L -0.02 Spiked Amount 40.000 Recovery 76.08%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.83 74 132664 9.36 ug/1 96 3) bis(2-Chloroethyl)ether 11.56 93 252667 13.74 ug/1 95 4) 1,3-Dichlorobenzene 12.07 146 209041 11.99 ug/1 97 5) 1,4-Dichlorobenzene 12.20 146 220513 11.56 ug/1 99 6) 1,2-Dichlorobenzene 12.73 146 216060 13.01 ug/1 98 7) 2,21 -oxybis(1-Chloropropan 13.05 45 515895 14.47 ug/1 98 8) N-Nitrosodi-n-propylamine 13.43 70 185149 14.10 ug/1 97 9) Hexachloroethane 13.57 117 60521 8.92 ug/1 99 11) Nitrobenzene 13.84 77 208460 12.47 ug/1 98 12) Isophorone 14.49 82 516603 15.77 ug/1 97 13) bis(2-Chloroethoxy)methane 15.17 93 302600 14.26 ug/1 99 14) 1,2,4-Trichlorobenzene 15.68 180 180141 12.60 ug/1 99 15) Naphthalene 15.85 128 631368 14.90 ug/1 99 16) Hexachlorobutadiene 16.40 225 66944 10.12 ug/1 99 18) Hexachlorocyclopentadiene 18.60 237 11881 2.08 ug/1 95 19) 2-Chloronaphthalene 19.36 162 381376 15.46 ug/1 98 20) Dimethylphthalate 20.45 163 461194 14.85 ug/1 99 21) 2,6-Dinitrotoluene 20.67 165 66883 10.07 ug/1 98 22) Acenaphthylene 20.63 152 600654 13.67 ug/1 100 23) Acenaphthene 21.19 153 397284 15.17 ug/1 100 24) 2,4-Dinitrotoluene 21.83 165 76448 10.68 ug/1 93 25) Diethylphthalate 22.59 149 449708 16.17 ug/1 99 26) 4-Chlorophenylphenylether 22.74 204 199974 14.55 ug/1 99 27) Fluorene 22.71 166 432307 15.65 ug/1 98 29) Azobenzene 23.21 77 465135 13.51 ug/L 96 31) N-Nitrosodiphenylamine 23.13 168 155794 16.39 ug/1 93 32) 4-Bromophenylphenylether 24.21 248 110601 14.70 ug/1 99 33) Hexachlorobenzene 24.64 284 132773 15.45 ug/1 97 34) Phenanthrene 25.62 178 557313 15.27 ug/1 100

(#) = qualifier out of range (m) = manual integration REFI.D GCMS0510.M Mon May 13 09:06:06 2002 Page 1

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