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GCMS analysis results for sample AE08487, May 2002

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Laboratory report showing GCMS analysis of sample AE08487 conducted on May 16, 2002.

NYC-WTC_000023292–000023303

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAY0902\8487.D Vial: 12 Acq On : 10 May 2002 1:12 am Operator: Sample : GC/MS SCAN 5/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 10 13:54 2002 ।Quant Results File: GCMS0510. Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:59:40 2002 Response via : Initial Calibration DataAcq Meth

Internal Standards : GCMS0507

R.T. Qlon Response N Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 492286 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1797004 40.00 ug/1 0.00 17) Acenaphthene-diO 21.13 164 978758 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1371903 40.00 ug/1 0.00 3 8) Chrysene-d12 33.63 240 848765 40.00 ug/1 0.00 44) Perylene-dl2 37.87 264 536281 40.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 23.28 209 156013 32.05 ug/L 0.00 Spiked Amount 40.000 Recovery 80.12%

Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isopho rone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 194 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 495 N.D. 26) 4-Chlorophenylphenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 • N.D. 31) N-Nitrosodiphenylamine 23.28 168 375 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.57 178 369 N.D. (#) = qualifier out of range (m) = manual integration 8487.D GCMS0510.M Fri May 10 13:55:03 2002 Page 1

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