GCMS scan report for Method 508, April 2002

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Operator ID: Nefliu Date Acquired: 19 Apr 2002 4:00 pm Data File: C:\MSDCHEM\l\DATA\020419\08271.D Name: sample Mise: Method: C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title: Method 508 GC/MS Scan Library Searched: C:\DATABASE\nist98.1

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone V Heptane 3.13 0.3 ug/1 374840 1 11.38 52443900 40.0 N-Ethylformamide 6.12 0.4 ug/1 532735 1 11.38 52443900 40.0 Phenanthrene , 9-m. . . 31.09 0.4 ug/1 754247 4 31.72 82413200 40.0 Phenanthrene - dl 0 31.96 0.5 ug/1 1113170 4 31.72 82413200 40.0 2-Chloroethanol 33.00 0.2 ug/1 427914 4 31.72 82413200 40.0 ' —=-e-1, 4-diol 33.83 0.2 ug/1 430857 4 31.72 82413200 40.0 _ ropyne 36.56 0.2 ug/1 386547 5 39.93 73817600 40.0 Oxirane , e t henyl - 40.30 0.2 ug/1 372943 5 39.93 73817600 40.0 3-Azabi cyclo [3.3.... 40.44 0.2 ug/1 437878 5 39.93 73817600 40.0 1,2-Benzisothiazo. . . 40.53 0.2 ug/1 391524 5 39.93 73817600 40.0 1-Hep t ade c anami ne 41.16 0.2 ug/1 448172 5 39.93 73817600 40.0 -3-Butyn -1 - o l 42.32 0.2 ug/1 351838 6 43.16 65411100 40.0 4-Pluoro-3-nitrob. . . 45.18 0.2 ug/1 344965 6 43.16 65411100 40.0 Propane 2-Methyl-1, 5- (4H) . . . 45.62 0.3 ug/1 549678 6 43.16 65411100 40.0 46.32 0.3 ug/1 480945 6 43.16 65411100 40.0

08271.D SCANAPR0902.M Mon Apr 22 15:45:31 2002 Page 29

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