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GCMS analysis results for sample AE08271, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting the detection of unknown compounds and surrogate recovery in sample AE08271 on May 16, 2002.

NYC-WTC_000023255–000023265

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0902\8271.D Vial: 9 Acq On 9 May 2002 10:13 pm Operator: Sample GC/MS SCAN 5/8 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 10 13:51 2002 Quant Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 10 09:59:40 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 515961 40.00 ug/1 0.00 10) Naphthalene-d8 15.82 136 1894505 40.00 ug/1 -0.01 17) Acenaphthene-diO 21.14 164 1033021 40.00 ug/1 0.00 30) Phenanthrene-diO 25.57 188 1444384 40.00 ug/1 0.00 38) Chrysene-dl2 33.64 240 868292 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 509301 40.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 23.27 209 177044 34.45 ug/L 0.00 Spiked Amount 40.000 Recovery 86.13%

Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 897 N.D. 26) 4-Chlorophenylphenylether 0.00 204 . 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.28 168 373 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.58 178 483 N.D.

(#) = qualifier out of range (m) = manual integration 8271.D GCMS0510.M Fri May 10 13:52:24 2002 Page 1

NYC-WTC_000023257

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NYC-WTC_000023257Source: NYC Law Department, mirrored locally

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