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GCMS analysis results for sample AE09571, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.

NYC-WTC_000023023–000023054

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 13 11:45:51 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) . Title : 508 Modified GC/MS scan XN Last Update : Mon May 13 11:40:29 2002 0/ Response via : Initial Calibration /J ’ DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.94 152 8239705 40.00 ug/L 0.01 10) Napthalene-d8 13.44 136 32626405 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.57 164 17678487 40.00 ug/L 0.00 29) Phenanthranene-dlO 22.96 188 25746404 40.00 ug/L 0.00 37) Chrysene-dl2 30.81 240 19973180 40.00 ug/L 0.00 43) Perylene-dl2 34.71 264 14267304 40.00 ug/L 0.00

System Monitoring Compounds 27) TCMX 20.55 209 3675394 34.24 ug/L 0.00 Spiked Amount 40.000 Recovery 85.60%

Target Compounds Qvalue 2) n-nitros-dimethyl amine 3.57 74 18834 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-nitroso-di-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Napthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) 2-Chloronaphthalene 0.00 162 0 N.D. 19) Dimethylphthalate 0.00 163 0 N.D. 20) 2,6-Dinitrotoluene 0.00 165 0 N.D. 21) Acenapthylene 0.00 152 0 N.D. 22) Acenapthalene 0.00 153 0 N.D. 23) 2,4-Dinitrotoluene 0.00 165 0 N.D. 24) Diethylphthalate 0.00 14 9 0 N.D. 25) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 26) Fluorene 0.00 166 0 N.D. 28) Azobenzene 20.55 77 62332 N.D. 30) Nnitrosodiphenylamine 20.55 169 72793 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 25.09 149 44467 N.D.

(#) = qualifier out of range (m) = manual integration 9570.D 050102.M Mon May 13 11:46:23 2002 Page 1

NYC-WTC_000023025

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