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GCMS analysis results, sample AE09154, May 2002

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GCMS analytical report for environmental sample AE09154 including surrogate compound data from May 15, 2002.

NYC-WTC_000022819–000022849

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022824
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OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.290 31 36 43 PV 12995 201048 0.43% 0.072% 2 3.349 43 46 54 W 6 4132 68113 0.14% 0.024% 3 3.520 68 75 80 PV 6 2186 33462 0.07% 0.012% 4 3.584 80 86 95 W 13947 236396 0.50% 0.085% 5 3.719 100 109 115 W 5 6540 229643 . 0.49% 0.082%

6 3.766 115 117 119 W 3 3589 36419 0.08% 0.013% 7 3.807 122 124 130 W 6 3081 62347 0.13% 0.022% 8 4.230 192 196 201 W 4 2518 37382 0.08% 0.013% 9 5.018 321 330 335 PV 7 5234 135186 0.29% 0.048% 10 5.077 335 340 355 W 9 5715 196243 0.42% 0.070%

11 5.394 388 394 399 W 4 3443 77282 0.16% 0.028% 12 5.576 417 425 429 W 8 2373 63141 0.13% 0.023% 13 5.641 429 436 447 W 5 3031 84132 0.18% 0.030% 14 5.964 483 491 521 PV 705604 13001069 27.53% 4.651% 15 7.450 738 744 750 PV 7 2145 43351 0.09% 0.016%

16 7.726 786 791 807 PV 3 9306 273595 0.58% 0.098% 17 8.737 955 963 968 W 7 2103 40513 0.09% 0.014% 18 8.819 972 977 985 W 5 3336 70265 0.15% 0.025% 19 9.301 1054 1059 1078 W 5 2350 77300 0.16% 0.028% 20 9.930 1147 1166 1186 PV 1703938 32754709 69.36% 11.717%

21 10.077 1186 1191 1204 VB 9 1662 44311 0.09% 0.016% 22 11.869 1490 1496 1502 W 5 2200 36745 0.08% 0.013% 23 12.045 1518 1526 1529 W 5 1868 40766 0.09% 0.015% 24 12.662 1626 1631 1637 PV 6 2071 39633 0.08% 0.014% 25 13.432 1749 1762 1781 W 2366866 43705396 92.55% 15.634%

26 13.579 1781 1787 1795 W 2 7618 150649 0.32% 0.054% 27 14.260 1895 1903 1909 W 8 2423 43793 0.09% 0.016% 28 15.694 2143 2147 2155 W 6 2040 40848 0.09% 0.015% 29 16.745 2319 2326 2337 BV 4 3826 79886 0.17% 0.029% 30 17.145 2390 2394 2401 PV 3 7356 104261 0.22% 0.037%

31 17.662 2475 2482 2489 PV 5 3575 63005 0.13% 0.023% 32 18.567 2625 2636 2654 PV 2457188 47223522 100.00% 16.892% 33 18.684 2654 2656 2661 W 4 1333 15792 0.03% 0.006% 34 18.961 2696 2703 2710 PV 6 1920 40981 0.09% 0.015% 35 20.541 2960 2972 2985 PV 1169047 22535607 47.72% 8.061%

36 21.393 3112 3117 3126 PV 4 9209 145342 0.31% 0.052% 37 22.580 3310 3319 3327 PV 2 18516 336142 0.71% 0.120%

9154.D 050102.M Mon May 13 11:28:43 2002 Page 1

NYC-WTC_000022824

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NYC-WTC_000022824Source: NYC Law Department, mirrored locally

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