GCMS reference standard results, sample AE09331, May 2002

z 2 K Quantitation Report (QT Reviewed) - O o 2 Data File Acq On : C:\MSDCHEM\1\DATA\050902\508REF2.D Vial: 17 CD — o : 10 May 2002 5:09 am Operator: Mclean "0 I o Sample : 5/8 eh Inst : Instrumen C O o o o Mise : Multiplr: 1.00 o' N MS Integration Params: EVENTS.E "0 N o Quant Time: May 13 9:49 2002 Quant Results File: 050102.RES — C 0 O Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) o Q C Title : 508 Modified GC/MS scan 3 Last Update : Mon May 13 09:45:43 2002 CD

Response via : Initial Calibration Abundance TIC: 508REF2.D

3200000 o o s8 3000000 T z s § s c 2800000 % I(! g c

2600000 8 £ 2 CM 8 2 2400000 § o £ 2200000 £ 2000000 $:

i CM 1800000 Ji O 8 G B 0) z8 1600000 2W J o2sl3 o 2 s I II t £ es 62 5 g h 2 1400000

1200000 g sh J 2 i 2

e II 2Q § 2o 5 8« 1111 8 g ° 2 E 2 1 d

Aulkge. HI95wo 1 1 2. 1000000 2 N a 858= « £ 2 2 £o N "eo f 1 % 8 8 1 18 o- 800000 1 Q - ” 848 % a 88 9a O 8 § CD 2$ ! I 3 11 1 600000 N o E g 8 400000 o CD & if ! 200000

Time-> O-r 4.00 4 IL . 6.00 8.00 1 I | l| .J Jill, , — ,. | 1 1 10.00 — 12.00 14.00 j 16.00 18.00 20.00 22.00 A..,i I 24.00 26.00 1 28.00 30.00 IL,, UUI 111 • 32.00 r11BT 34.00 36.00 38.00

508REF2.D 050102.M Mon May 13 09:49:49 2002 Page 3