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GCMS blank analysis for sample AE11604, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank test results for nitrosamines and other compounds in sample AE11604 analyzed May 21, 2002.

NYC-WTC_000022622–000022629

Folder label: “GCMS X 5/20/02 A 5/22/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C: \HPCHEM\ 1 \DATA\MAY210 2 \ LBA. D Vial: 28 Acq On : 22 May 2002 5:09 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.109 332 335 365 rVB 486831 1147499 35.55% 6.572% 2 12.141 769 775 791 rBV 1042918 2457950 76.15% 14.076% 3 15.779 1166 1172 1190 rBV 1490782 3188456 98.78% 18.260% 4 21.085 1745 1751 1769 rBV 1584902 3227816 100.00% 18.485% 5 23.229 1975 1985 1991 rBV 779675 1598975 4.9.54% 9.157% 6 25.529 2229 2236 2248 rBV2 1323139 2778943 86.09% 15.915% 7 33.575 3108 3114 3131 rBV2 792013 1762624 54.61% 10.094% 8 37.781 3566 3573 3591 rBV2 436043 1299158 40.25% 7.440%

Sum of corrected areas: 17461421 LBA.D GCMS0520.M Fri May 24 08:35:05 2002

NYC-WTC_000022626

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NYC-WTC_000022626Source: NYC Law Department, mirrored locally

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