NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAY2102\LBA.D Vial: 28
Acq On : 22 May 2002 5:09 pm Operator:
Sample : EXTRACTS/20 Inst : 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: May 24 8:10 2002 Quant Results File: GCMS0520.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon May 20 15:10:30 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0520
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.14 152 402070 40.00 ug/1 0.00
10) Naphthalene-d8 15.78 136 1573043 40.00 ug/1 -0.01
17) Acenaphthene-diO 21.09 164 755400 40.00 ug/1 0.00
30) Phenanthrene-diO 25.53 188 983256 40.00 ug/1 0.00
38) Chrysene-dl2 33.57 240 541716 40.00 ug/1 -0.03
44) Perylene-dl2 37.78 264 341062 40.00 ug/1 -0.02
System Monitoring Compounds
2 8) TCMX 23.23 209 148923 39.23 ug/L 0.00
Spiked Amount 40.000 Recovery 98.07%
Target Compounds Qvalue
2) N-nitrosodimethylamine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 12.05 146 442 N.D.
5) 1,4-Dichlorobenzene 12.19 146 351 N.D.
6) 1,2-Dichlorobenzene 12.71 146 105 N.D.
7) 2,2'-oxybis(1-Chicropropan 0.00 45 0 N.D.
8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.54 117 222 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Is ophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.83 128 346 N.D.
16) Hexachlorobutadiene 16.37 225 526 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenylphenylether 23.23 204 624 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzene 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 23.23 168 233 N.D.
32) 4-Bromophenylphenylether 0.00 248 0 N.D.
33) Hexachlorobenzene 0.00 284 0 N.D.
3 4) Phenanthrene 0.00 178 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBA.D GCMS0520.M Fri May 24 08:10:49 2002 Page 1
NYC-WTC_000022623
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