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GCMS results for sample AE11481, May 29, 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS analysis for sample AE11481 conducted on May 29, 2002.

NYC-WTC_000022575–000022587

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020521\11481.D Vial: 15 Acq On : 21 May 2002 10:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 09:35:51 2002 Quant Results File: SCAN020521.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Fri May 24 09:17:56 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 422580 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1603088 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 866580 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1465103 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1134087 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 637658 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.56 207 236990 34.10 ug/1 -0.04 Spiked Amount 40.000 Recovery 85.25% Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 11481.D SCAN020521.M Fri May 24 09:37:10 2002 Page 1

NYC-WTC_000022577

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NYC-WTC_000022577Source: NYC Law Department, mirrored locally

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