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Document / 9 pages

GCMS method parameters and calibration data, May 2002

Machine-extracted title · confidence 95%

Technical log detailing gas chromatography mass spectrometry method parameters and calibration settings from May 2002.

NYC-WTC_000022495–000022503

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\020521\0517LB1.D Vial: 3 Acq On : 21 May 2002 10:15 am Operator: Nefliu Sample : 05/17 lab blk kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 6.152 518 523 563 rBV 440881 933862 23.55% 4.097% 2 11.370 1399 1411 1432 rBV 1116287 2861894 72.16% 12.554% 3 16.534 2276 2290 2310 rBV 1393490 3586818 90.44% 15.734% 4 24.460 3622 3639 3661 rBV 1370429 3743198 94.39% 16.420% 5 27.551 4146 4165 4183 rBV2 ' 846946 2367962 59.71% 10.387% 6 31.088 4758 4767 4780 rBV4 8262 28700 0.72% 0.126% 7 31.717 4857 4874 4899 rBV2 1301868 3965832 100.00% 17.397% 8 31.952 4907 4914 4925 rVB5 9482 26723 0.67% 0.117% 9 39.931 6260 6272 6303 rBV2 1648546 3159337 79.66% 13.859% 10 43.151 6810 6820 6852 rBV2 994734 2121968 53.51% 9.308%

Sum of corrected areas: 22796294

0517LB1.D .SCAN020521.M Fri May 24 09:13:22 2002 Page 1

NYC-WTC_000022498

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NYC-WTC_000022498Source: NYC Law Department, mirrored locally

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