Volatile organic compounds analysis results, March 21, 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\02mar21\6580F.D Vial: 12 Acq On : 22 Mar 2002 12:17 am Operator: 201-wb Sample : fb Inst : GC/MS Ins Mise : March 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Nonanol Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 28.09 0.13 ug/L 73156 1,4-DICHLOROBENZENE-D4 26.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Nonanol 144 C9H20O 000143-08-8 35 2 1-Octanol 130 C8H180 000111-87-5 27 3 IH-Pyrrole, 2,5-dihydro-l-nitroso- 98 C4H6N2O 010552-94-0 25 4 1-Heptene 98 C7H14 ______ 000592-76-7 25 Abundance Scan 1416 (28.092 min): 6580F.D (-) m/z 41.05 100.00% 41 8000

6000 57

4000 67 82 27.80 28.00 28.20 28.40 — 98 m/z 57.05 60.72% ■ i ■'' ■ i' ‘ ‘ ■ i * i * * TTt ■ ‘ i ■ ■ •' i' ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #66370:1-Nonanol 41 55

70 5000 27.80 28.00 28.20 28.40 83 m/z 55.05 53.62% 98 | 11111' i ■ ■' ■ i ■' 126 11)1 ‘ *' i *' '111 ‘' i ■' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #65277:1-Octanol 41 56 27 ' ‘ I 1 ■ ■ ■ i ' ■ i ■ ■ ‘ ■ i ■ ■ 27.80 28.00 28.20 28.40 m/z 44.05 53.08% 5000 69 84

m/z-> Abundance • ।1 * * * । *' * • । • ■ i ■ ■ — rq-r ■ ■ i ■ ■ ■11'' ■ ■ i ■ ■111 ' ■ ■11 ■ ■ 20 30 40 50 60 70 80 90 100 110 120 130

41 #1199: 1H-Pyrrole, 2,5-dihydro-1-nitroso- Q 27.80 28.00 28.20 28.40 m/z 43.05 50.64%

5000 98 30 67 57

/z-> T-p-rT 20 30 40 44 i ‘ ‘' i'1 ■ ‘ i'' 50 60 70 80 90 100 110 120 130 i''1 ■ i' ■' ■ i 11 • ‘ '1 i' ‘■ I ■ ■ ■ ' i ' ■ ' ' i ‘ ' 27.80 28.00 28.20 28.40

6580F.D HP031802.M Fri Mar 22 00:56:39 2002 Page 1

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